Pour the contents of one of the test tubes into the other and a reaction should occur and you should see a white precipitate of barium sulfate form. Then, centrifuge it for 1 minute. On the side, weight a boiling test tube containing 2 boiling chips. When the separation is complete, remove the small test tubes from the centrifuge and decant the supernatant into the boiling test tube. Add 1 mL of deionized water to the small test tube containing the precipitate and mix it and centrifuge it for 60 seconds.
Allow the mixture to cool for a few minutes then filter it, using either gravity or vacuum filtration. (We shall be using vacuum filtration.) Wash the residue in the funnel once with a little water and collect all the filtrate. 4. Pour all the filtrate and washings into a 250cm3 volumetric flask.
Then you put the remaining liquid (neutral component mixture) through the suction filtration funnel to isolate the crystals. After 10-15 minutes, the crystals will be dry and you can weigh them and find their melting point. How is the neutral component of your 3-compound mixture isolated from the final methylene chloride solution? 16 of 22 4/16/12 9:15 PM StudyBlue Flashcard Printing of Lab Final 2211L UGA http://www.studyblue.com/servlet/printFlashcardDeck?deckId=... Name the four active ingredients that we will be testing for in the TLC of Analgesics lab: Ibuprophen Caffeine Acetaminophen Acetylsalicylic acid What solvent system will you be using to dissolve the common analgesics (power) in preparation for TLC spotting? Methylene chloride: ethanol (1:1 solution) What solvent system will you be using to "develop" your TLC plates in the TLC of Analgesics lab?
Materials and Methods Part 1 For the cation elimination test first 10 drops of potassium, iron (III), zinc (II), copper (II), and cobalt (II) were added to 5 centrifuge tubes and the color was recorded. Then for the metal hydroxide test, 6 M NaOH was added drop wise till a precipitate was formed. Each solution except potassium formed a precipitate, so then 10 additional drops of NaOH were added to the remaining solutions. Tubes were cleaned with distilled water and 6 M HCL. Next was the ammonia test 10 drops of each metal solution were added to new centrifuge tubes and 15 M NH4OH was added until the solution changed color or a precipitate was formed.
Reactions Lab David Vaghari INSTRUCTOR: Dr. Chernovitz Monday, July 23, 2012 Oxygen Production Introduction In this lab, potassium chlorate will be decomposed producing oxygen gas and potassium chloride. The hypothesis is that the reaction will yield 3.916 grams of oxygen gas. Materials Test tube 10 grams potassium chlorate Bunsen burner Procedure Step 1. Obtain a test tube, place a 10 gm of potassium chlorate. Step 2.
Part C: Density of Sodium Chloride (NaCl) Solution, a sample of NaCl was obtained and measured using a 100mL beaker and a 10mL pipet to determine the concentration of the solution. In order to obtain the appropriate result, a calibration graph and density measurement was used to determine the concentration of the sodium chloride solution. In conclusion, based on the water temperature of 21.8°C in part A’s graduated cylinder experiment obtained, it was determined that the average density was .0973g/mL with a percentage error of 2.5%. When graphed the measurement was equal to Y=0.988x. Part B: The graduated pipet’s average density at 22.3 °C was determined to be 0.9785g/mL with a percentage error of 1.89% shows the graduated pipet to be more accurate and precise.
Experiment#2 “Separating the Components of a Ternary Mixture” By Mohammad Bazargan Lab partners: Aaron Radtke, Kevin Campbell, Austin Gilchrist Instructor: Professor Mundell Section #: 12 Sep/14/2011 Abstract In this laboratory, we used physical and chemical properties to separate the components of a ternary (three substances) mixture. We also determine the percentage of each substance in the mixture. The percentages are the following,38.2% NaCl, 40.45% SiO2, and 72.84% CaCO3.The mentioned substances were all separated using methods such as filtration, evaporation and reaction with other chemicals which will be explained throughout this report. Intro Mixtures are \ physical combinations of two or more substances where each substance keeps its own chemical identity. Mixtures can be classified as either homogeneous or heterogeneous.
0.9 0.8 0.7 Absorbance 0.6 0.5 0.4 0.3 0.2 0.1 0 400 450 500 550 600 650 700 750 λ max 500 nm 550 nm • • Make sure you understand the directions for using the spectrophotometer and have them written in your manual. Complete the questions on the prelab page. Introduction: There are many different chemical methods that can be used to determine the concentration of a solution. You have already used one method, titration, to find the concentration of Ca+2 ions in a sample of water, and another, density, in finding the concentration of ethanol. In this lab you will use a method called visible spectroscopy to determine the concentration of a solution of CoCl2.
Once you have calculated the amount of each reactant, proceed to the lab table and retrieve the following equipment: two graduated cylinders, two beakers, two flasks, funnel, and filter paper. Take the mass of the filter paper. Pour the right amount of each reactant, into the two beakers. From
1) Jeffrey Cox CHE111-DL01 Lab number 10 Stoichiometry of a Precipitation Reaction 2) Purpose/ Intro. In this lab we will be able to calculate the actual, theoretical, and percent yield of the product from a precipitation reaction. We will thusly learn the concepts of solubility and the formation of a precipitate. A precipitate reaction is a reaction in which soluble ions in separate solutions are mixed together to form an insoluble compound that settles out of the combined solution as a solid. The solid then is the insoluble compound, called a precipitate.