Make sure to keep time, read the spectrometer, and record the data. Note time to the nearest second and mix the contents of tubes 2 and 3 by pouring them back and forth twice. Mixing should be completed within ten seconds. 5) Add the reaction mixture to a cuvette by pouring or using eye dropper, wipe the outside, and place the cuvette in the spectrometer. Read the absorbance at 20 second intervals from the start of the mixing.
Add 1 mL of deionized water to the small test tube containing the precipitate and mix it and centrifuge it for 60 seconds. Then, add the supernatant into the boiling test tube and repeat this step one more time with another 1 mL of deionized water. Acquire a pair of metal test tube holders and heat the boiling test tube to evaporate the water for 15 minutes. Let is cool after and weigh it. Then, calculate a percent yield of zinc iodide and write a balanced chemical equation and determine the limiting
Using a test tube holder, heat the R tube over the Bunsen burner, moving the tube in a circular motion until all the water has evaporated. The P tube will be carefully heated next, for about 10 minutes, until all the water has evaporated, and there is a white substance in the tube. After the water has evaporated, continue heating the tube over the burner for a minute longer, being careful to watch out for purple gas and yellow spots. The P tube
B. The effect of pH changes Place about 1 mL of 2% albumin in each of four test tubes. Add 3 mL of water to the first. This tube will serve as a control. To the second, add 10% NaOH dropwise until the pH is 14.
Experimental First, we weighed 2 samples, each has 1 gram of NaHCO3-KCl mixture Second, we put the samples in 2 crucibles (A and B) and weighed them. (crucible + sample; WA1 and WB1) Third, we heated both samples on a hot plate for 30 minutes. Fourth, we weighed the samples again (crucible + sample; WA2 and WB2) Lastly, we determined NaHCU3 percentage in the mixture using the following method: WA1 – WA2 x 100% 0.309 WA1 – WA2 x 100% 0.309 * * Results * Theorectically: * Discussion When sodium hydrogen carbonate is heated, new products are formed; sodium carbonate, water vapor, and carbon dioxide gas. This reaction may be presented in a different form with a measure of molecules: @Na2CO3 + H2O + CO2 (solid) (solid) (gas) (gas). Once the reaction of sodium hydrogen carbonate takes place, carbon dioxide gas is released, as well as water vapor.
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Reactions Lab David Vaghari INSTRUCTOR: Dr. Chernovitz Monday, July 23, 2012 Oxygen Production Introduction In this lab, potassium chlorate will be decomposed producing oxygen gas and potassium chloride. The hypothesis is that the reaction will yield 3.916 grams of oxygen gas. Materials Test tube 10 grams potassium chlorate Bunsen burner Procedure Step 1. Obtain a test tube, place a 10 gm of potassium chlorate. Step 2.
The following data were obtained when a sample of barium chloride hydrate was analyzed as described in the Procedure section. Calculate (a) the mass of the hydrate, (b) the mass of water lost during heating, and (c) the percent water in the hydrate. Mass of empty test tube 18.42 g Mass of test tube and hydrate (before heating) 20.75 g Mass of test tube and anhydrous salt (after heating) 20.41 g. Mass of the Hydrate is 2.33g. Loss (H2O) is 0.34g. Percent H2O in Hydrate is equal 0.34/2.33=14.6% 3.
pyridinium hydrobromide perbromide type of stationary phase column length column temperature rate flow of the carrier gas List the 4 general factors that affect the separation obtained on a gas chromatograph What specific technique is used to collect/isolate your purified unknown compound at the end of the recrystallization experiment? suction filtration 14 of 22 4/16/12 9:15 PM StudyBlue Flashcard Printing of Lab Final 2211L UGA
The liquid of homogenate was filtered into a beaker through Miracloth (2 layers cloth) to remove large plant components and 1 ml of the filtrate was transferred to a conical tube. 8.4 g of ammonium sulfate was slowly added to the 40 ml of the filtrate as it was stirred on a stir plate for 15 min to achieve 37% saturation (210g/L of solution). The solution was then centrifuged at a speed of 9000 x g at 4oC for 15 min to sediment the proteins. The resultant supernatant 1 was transferred to a beaker with 1 ml transferred to a conical tube and the obtained pellet 1 was resuspended in 4 ml of distilled water and transferred into a dialysis bag to remove the salt. Then, 3.4 g of ammonium sulfate was slowly added to the supernatant 1 as it was stirred for 15 min to achieve 50% saturation (85g/L of solution).