Observing Changes – Materials & Procedures Materials Water Copper (II) sulphate (Powder) Copper (II) sulphate solution Iron nail Sodium carbonate Hydrochloric acid Magnesium ribbon Flame (candle) Sugar Aluminum foil Test tubes Test tube rack Tongs Medicine dropper Spoons Beakers Safety goggles Scoopulas Procedures Water and Copper (II) Sulphate Procedure 1. Add a small amount of solid copper (II) sulphate to a test tube with a scoopula. Record the physical properties. 2. Write a hypothesis on what you think will happen when water is added.
0.9 0.8 0.7 Absorbance 0.6 0.5 0.4 0.3 0.2 0.1 0 400 450 500 550 600 650 700 750 λ max 500 nm 550 nm • • Make sure you understand the directions for using the spectrophotometer and have them written in your manual. Complete the questions on the prelab page. Introduction: There are many different chemical methods that can be used to determine the concentration of a solution. You have already used one method, titration, to find the concentration of Ca+2 ions in a sample of water, and another, density, in finding the concentration of ethanol. In this lab you will use a method called visible spectroscopy to determine the concentration of a solution of CoCl2.
2 marks 4 Draw the structural formula of Compound G. 1 mark 5 Using the chemical shift correlation for 13C NMR, predict the number of peaks for Compound G and draw in the position of the peaks on the blank spectrum below, annotating each peak with its corresponding structure. (2 marks) 6 Draw the structural formula for 2-chloro but-2-ene. Below this draw a structural formula of an isomer of 2-chloro but-2-ene and name this substance.
How do you go from calculated/measured values to accomplishing stated purpose? (4 pts) The purpose of this lab is to determine the exact concentration of an unknown acetic acid solution. Titrations for two different reactions will be performed. Controlled volumes of one reagent are added to a flask containing the other reagent until the equivalence point of the reaction is reached, one between sodium hydroxide (NaOH) and potassium hydrogen phthalate (KHP) and the other between NaOH and acetic acid (CH3COOH). NaOH (aq) + KHP (aq) —› Na+ (aq) + K + (aq) + P2- (aq) + H2O (l) NaOH (aq) + CH3COOH (aq) —› Na+ (aq) + CH3COO- (aq) + H2O (l) The titration of NaOH with KHP will identify the concentration of the NaOH provided.
CHEM 3210 SEC 318 November 12, 2013 Nucleophile Substitution Reactions of Alkyl Halides Summary: Nucleophilic substitution can occur by an SN1 mechanism or an SN2 mechanism. In SN1 and SN2 reactions, the reaction rate is affected by: the nature of the halide, the nature of the solvent, the reaction temperature, the nature of the nucleophiles, and the concentration of reactants. In this experiment we will be examining reactions with NaI/acetone and AgNO3/Ethanol. We will determine the relative rates of reaction and determine whether these substances can undergo an SN2 reaction. Halides Structure BP 1-Chlorobutane 77-78°C 1-Bromobutane 100-104°C 2-Chlorobutane 68-70°C 2-Chloro-2-methylpropane 51-52°C Bromobenzene 156°C 1-Chloro-2-butene (trans) 68°C 1-Chloro-2-butene (cis) 63.5°C 1-Chloro-2-methylpropane 68-69°C 2-Bromobutane 91°C 2-Bromo-2-methylpropane 71-73°C Procedure: 1.
| | | An Activity Series 1/9/13 Makieya DunhamPartners: Jasmine Lewis and Danielle Anderson | | | Problem Statement: In this lab we determined the activity series for five metals and for three halogens. In the first part of the lab we used a microscale technique to rank the metals that reacted with the other metal nitrates from most reactive to least reactive. The metal that reacts with another metal nitrate, then the solid metal have reduced the other metal ion and is the more reactive metal of the two. In the second part of the lab we used the solvent extraction technique to derive an activity series for the halogens. Safety Precautions: When in the lab we wore goggles, an apron, and gloves the entire time.
Abstract The focus of this experiment was to analyze the kinetics of a nucleophilic substitution. A mixture of 0.3622-M 1-bromopropane and 0.3622-M potassium hydroxide in an 90:10 ethanol/water solvent provided the reactants for a SN2 reaction to occur in a temperature controlled bath at 50.0˚C. The disappearing reactant was found by titrating timed aliquots during the reaction and then measuring the concentration of hydroxide. The k-value was found to be 0.0202 M-1Min-1. Using the linear form of the Arrhenius equation the activation energy was calculated to be 19.9 kcal/mol.
Exothermic and endothermic reactions. First law of thermodynamics and enthalpies of reactions. Calculate standard enthalpies of formations (using the equation on page 191). Electromagnetic radiation, photoelectric effect and continuous and line spectra. Energy levels and electron configurations (including representation using orbital diagrams) of several common elements on the periodic table.
Alex Pascal Lab Partners: November 12, 2009 Period 8 Periodicity in the Properties of Some Representative Elements Purpose: The purpose of this lab was to if elements in the same family react similarly. Procedure: A) A test tube, test tube rack was acquired. A small amount of HCl was measured in a graduated cylinder and poured into test tube. Then a bunsen burner, a small amount of Mg ribbon and a wooden splint was acquired. The Mg ribbon was then placed in HCl in the test tube and observed.
Title: Bromination of (E) – Stilbene (Microscale Procedure) Author’s Name: Reinaldo George Professor: Elvis Barrett Date of Experiment: Thursday July 16th 2015 Institution: Nova Southeastern University Abstract The purpose of this experiment was to synthesize the second intermediate in the b series of Sequential Reactions by carrying out the bromination of (E)-stilbene to obtain meso-stilbene dibromide. This product is the precursor to diphenylacetylene, the next synthetic intermediate in the b series. A further purpose of this experiment is to demonstrate the stereospecific addition of bromine to alkenes. The percentage recovery was also calculated and recorded. On completion of this experiment; my lab partners and I were able to successfully synthesize the second intermediate in the b series of the