6. Slowly add 2mL of sodium hydroxide (8M) to the beaker. Look for any solid that appears. 7. Heat the beaker on a hot plate set to medium.
Add 1 mL of deionized water to the small test tube containing the precipitate and mix it and centrifuge it for 60 seconds. Then, add the supernatant into the boiling test tube and repeat this step one more time with another 1 mL of deionized water. Acquire a pair of metal test tube holders and heat the boiling test tube to evaporate the water for 15 minutes. Let is cool after and weigh it. Then, calculate a percent yield of zinc iodide and write a balanced chemical equation and determine the limiting
Set min temperature to 15-18C c. Time should range from 0-250 seconds 7. Press DISPLAY to accept all values 8. Heat up 200mL of water in a microwave for about two minutes 9. Place hot water on a hot plate to keep warm 10. Nest one Styrofoam cup in another 11.
Using a test tube holder, heat the R tube over the Bunsen burner, moving the tube in a circular motion until all the water has evaporated. The P tube will be carefully heated next, for about 10 minutes, until all the water has evaporated, and there is a white substance in the tube. After the water has evaporated, continue heating the tube over the burner for a minute longer, being careful to watch out for purple gas and yellow spots. The P tube
5. Repeat until the mass is consistent. Data and Observations: Measured melting point | 93.0 ̊ C | Real melting point | 92.5 ̊ C | Mass of evaporating dish | 47.01 g | Mass of evaporating dish and crushed alum | 49.13 g | Mass of crushed alum | 2.12 g | Mass after 1st heating | 48.17 g | Mass after 2nd heating | 48.16 g | Mass of water driven off | .97 g | Mass of anhydrous alum | 1.15 g | Moles of H2O | .0539 moles | Moles of AlK(SO4)2 | .0045 moles | Mole ratio; H2O/AlK(SO4)2 | 12.0 | During the heating of the crushed alum in the hot water bath, the alum had liquefied. The boiling point temperature that was determined was 93.0 degrees Celsius. This process had taken a long time, but around 90 degrees
Materials: 3 beakers Thermometer 3 Alka-Seltzer tablets Stopwatch Mortar and pestle Source of hot water Ice cubes Graph paper Procedures: Hot water- Run water from the hot tap until it is hot as possible Fill beaker with 80 mL of hot water Use thermometer to take temperature of water. Record in data table. Remove 1 Alka-Seltzer tablet from package Drop into the water. Measure the time it takes for the tablet to completely dissolve. BE READY WITH THE STOPWATCH.
CaCO3 + 2HCl -----CaCl2 + CO2 + H2O ( Volume of acid added (L) ) (1.0mol/L) = moles acid added. Moles acid added - moles base added = moles acid that reacted. Moles of acid that reacted / 2 = moles CaCO3 present in sample. Final answer % CaCO3 3. Put exactly 5.0 mL of water in the 10.0 mL graduated cylinder.
Lab Report: Crystallization of phthalic acid from water (microscale) Abstract The 0.60 g of phthalic acid is put in a water solution, which is brought to a boil to dissolve the acid into water. After the solution was clear with just the rock visible the test tube solution is now cooled in ice and stirred till crystals appear. Excess water is then removed, then the adding of ethanol is done to separate the water from the crystals. Tube is then placed in a beaker of hot water which aids in the removal of the solvent. After drying the compound the percent recovery was found to be 70%.
A voltmeter was used to measure the electrical resistance of different solutions. * Experiment and Observation: The plastic and glassware used in this experiment was thoroughly washed with hot water and rinsed with distilled water. * * Part I: Preparation of Standard Phosphate Solutions 1. 1.0 ppm standard: 1.00 mL of 10.0 ppm phosphate solution was placed in a 25 mL graduated cylinder and diluted to exactly the 10 mL mark with distilled water then poured into a plastic cup labeled 1. Cylinder was rinsed with distilled water.
Obtain a clean-dry test tube. Place 0.3g of the unknown substance in the test tube. Next, add 10mL of distilled water to the test tube. Mix with a stirring rod until unknown is dissolved. 2.