Qualitative Analysis Of Common Anions

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Name: Razlan bin Mohamed Fitri Partner's Name: Vinod MenonExperiment 1: Qualitative Analysis of Common AnionsAim: To investigate the qualitative analysis of common anions.Procedure: Refer to lab manual page 18-20.Results: Procedure Number and Ion | Test Reagent or Technique | Evidence of Chemical Change | Chemical(s) Responsible for Observation | Equation(s) for Observed Reaction | 1) | Addition of 6M NH3 and 0.3M Ba(NO3)2 | Whole solution is precipitated | Ammonia,NH3 and Barium Nitrate, Ba(NO3)2 | | 2) | Centrifuging | Only precipitate left | | | 3) SO4 ²ˉ | Addition of 6M HNO3 and centrifuging | White precipitate undisolved | Barium sulphate, BaSO4 and Nitric acid, HNO3 | | 4) PO4 ³ˉ | Addition of 0.2M (NH4)6Mo7O24 and heating | Yellow precipitate is formed | Barium phosphate, Ba3(PO4) and Ammonium heptamolybdate, (NH4)6Mo7O24 | | 5) CO3 ²ˉ | Repeat Part A and addition of 6M HNO3 and insertion of stirring rod dipped in saturated Ca(OH)2 | Milky solution seen | Barium carbonate, BaCO3 and Calcium hydroxide, Ca(OH)2 | | 6) S ²ˉ | Addition of 6M HNO3 and 1M Cu(NO3)2 and centrifuging | Blackish green precipitate formed | Nitric acid, HNO3 and Copper (II) nitrate, Cu(NO3)2 | | 7) I ˉ | Addition of 0.2M Fe(NO3)2 and toluene | Purple color seen in toluene layer | Iron (III) nitrate, Fe(NO3)2 and toluene | | 8) Br ˉ | Addition of 6M HNO3 and 0.1M KMnO4 | Brown bromine seen in the toluene layer | Nitric acid, HNO3 and Potassium permanganate, KMnO4 | | 9) Cl ˉ | Addition of 0.01M AgNO3 | White precipitate formed | Silver nitrate, AgNO3 | | 10) | Addition of 6M NH3 | White precipitate dissolves at first, then turns black( which
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