Measure the solution by right clicking on the beaker and choose pH meter *Then I had to measure the pH of 0.1 M sodium hydroxide Get a 100 mL beaker from the equipment menu Right click on the beaker, select chemicals, and add 50 mL of 0.1 M sodium hydroxide. Measure the solution by right clicking on the beaker and choose pH meter Part 2: *First add 35 ml of unknown acid a to 100 mL beaker. Select all chemicals from the toolbar in the chemicals section, choose unknown acid a. Put the volume at 35 mL in a new 100 mL beaker. *Then add two drops of phenolphthalein indicator to the beaker by right clicking, choosing indications, and adding 2 drops of phenolphthalein.
In the chart provided record if each compound is solubility in water. Part D - Conductivity 1. Obtain six 100ml beakers and add 50ml of water to each. 2. Place a 10g sample of each of the above compounds in a separate beaker.
Next, 50 mL of distilled was placed into the 150 mL. Twenty drops of Bromothymol blue were added to the 150 mL beaker solution. The pH was then recorded. Five mL of this solution was transferred into three separate 100 mL beakers. In one of these beakers, 1 mL of HCl was added to the solution, making this the “Yellow” beaker.
Wait 90 seconds for the light source to warm up, then fill a cuvette with distilled water and clean the flat, clear sides on the cuvette with a Kimwipe, removing dust and fingerprints before putting the cuvette into the instrument. Orient the cuvette so that the clear sides line up with the white arrow on the top of the spectrometer. Click “Finish Calibration”, then “OK”. Next, fill a cuvette with the “yellow” sample, repeating the steps to clean the clear sides of the cuvette with a Kimwipe to remove fingerprints and dust. Place the clean cuvette containing the “yellow” sample into the spectrometer, orienting the cuvette so that the clear sides of the cuvette line up with the white arrow in the cuvette.
Each of the 3 unknowns was distributed by dispensing 2ml of sample solution in to three test tubes. Once in the test tube 400ug of each reagent was dispensed in the separate solutions. The test tube with Benedict ’s reagent was heated to 65 degrees C and let cool to see color change. The results from this test were then compared to our known nutrients and recorded in Table 2. Determining Absorbency of Starch To determine the absorbency of starch; a
Allow the mixture to cool for a few minutes then filter it, using either gravity or vacuum filtration. (We shall be using vacuum filtration.) Wash the residue in the funnel once with a little water and collect all the filtrate. 4. Pour all the filtrate and washings into a 250cm3 volumetric flask.
The buret had used the NaOH thoroughly rinsed three times because at the first titration the NaOH solution was used. About 50Ml the NaOH solution was in a clean beaker and brought it to experiment area. A funnel was used to fill the NaOH into the buret and recorded the initial volume on the buret to the correct number of significant figures. A pipette was used to take 10.00ml HCl into a clean 50mL Erlenmeyer flask. Three drops of phenolphthalein indicator was added into the HCl solution.
Why is this necessary? Obtain an appropriate amount of 5.00 M NaCl and fill your 25 mL buret. Pipet a 20.00 mL aliquot of 0.100 M acetic acid solution into a 100 mL beaker, add a magnetic stirring bar, and then set up the titration apparatus as indicated in Figure 1. Record the initial pH and then begin titrating. You will titrate in 0.25 mL intervals for the first 2 ml and then in 1 mL intervals until a total of 6 mL of 5.00 M NaCl has been delivered.
Place about 50mL of water in a beaker and 1 drop of the permanganate solution for the color constant. Record the initial volume reading in the buret. Add the permanganate to the FAS solution until the equivalence point is reached. Record the final volume reading in the buret. Repeat the process 2 more times.
Do this one more time the exact same, and then a third time using only 10 mL of the mixture. Each of the three times you do this, extract the liquid. Transfer the liquid into the large 100 mL round bottomed flask that is connected to your simple distillation set up. Distill the tomato paste liquid. Once it is completely distilled, remove your filtered material and add 2 mL of dichloromethane.