In order to find the concentration of NaOH we need to tag along the following steps: a- note down the balanced chemical equation for the reaction C8H5O5K+NaOH→C8H4O4KNa+H2O b- pull out applicable information from the experiment: C8H5O5K V=0.025 dm3 C=0.2M NaOH V=0.021 dm3 C= ?? c- calculate number of moles
Empirical formula: CH5N Steps for molecular formula: 1- Calculate the molar mass of the empirical formula. 2- Divide the known (given) molar mass by the calculated empirical formula molar mass to get a whole number 3- Multiply that whole number through subscripts of the empirical formula to obtain the molecular formula. Example CH5N 12.01 g C x 1 C= 12.01 g/mol 1.008 g H x 5 H = 5.040
Mirco-Scale Acid-Catalysed Iodination of Acetone. Abstract: The purpose of this experiment was to titrate different concentrations of HCl and ClCHCOOH against Na2S2O3. The volumes found were plotted against time and values for Kobs , KH+ and KHA were found from these graphs. The Kobs values found for each experiment were (i)Kobs = 2.48x10-6, (ii)Kobs = 6.2x10-7, (iii)Kobs = 5.3x10-7, (iv)Kobs = 4.6x10-7. The values found for KH+ for the reaction using HCl as the acid were found to be (i)KH+ = 4.96x10-5, (ii)KH+ = 1.24x10-5, (iv)KH+ = 1.84x10-5.
This solution was placed in a burette and 18.4 cm3 was required to neutralise 25 cm3 of 0.1 moldm-3 NaOH. Deduce the molecular formula of the acid and hence the value of n. 5. Sodium carbonate exists in hydrated form, Na2CO3.xH2O, in the solid state. 3.5 g of a sodium carbonate sample was dissolved in water and the volume made up to 250 cm3. 25.0 cm3 of this solution was titrated against 0.1 moldm-3 HCl and 24.5 cm3 of the acid were required.
The absorption spectrum is measured using a spectrophotometer and the data is graphed in Excel. The peak of the line is used to find Vmax of Fe2+. Vmax is used to find the moles of Fe2+ and ligand. The unknown n is a ratio of moles ligand divided by moles Fe2+. Results and Discussion For the first part of the experiment (Part A), five different 100 mL volumetric flasks were each filled with 1,2,3,4 and 5 mL of iron (II) solution.
EXPERIMENT 6 Title Kinetics of Chemical Reaction – Iodination of Cyclohexanone Aim To determine the value of the rate constant, k and order of reaction, a, b and c, and also to suggest a mechanism which agrees with the rate equation that has been obtained. Background Theory The basis of the theory of absorbance is as follows: Io ―――――→ sample ―――――→I if Io = I, no absorbance occur Io > I, the sample absorbs certain amount of light wave Io < I, the sample emits certain amount of light of certain wave length. THE HALOGENATION (IODINATION) OF KETONES (CYCLOHEXANONE) This experiment examined the rate of iodination of cyclohexanone in an aqueous medium. To increase the amount of iodine in the solution, iodine is converted to a more soluble complex ion, I3- by the addition of excess iodide ion: I2 + I- →I3- One of the characteristic reactions of ketones is the substitution of a halogen for one of the hydrogen is adjacent to the ketone group. The net reaction is: This reaction has been studied extensively and occurs for a wide variety of ketones.
Percent H2O in Hydrate is equal 0.34/2.33=14.6% 3. The general formula of barium chloride hydrate is BaClg-nHZO, where n is the number of water molecules. Calculate the theoretical percent water for each value of n—divide the sum of the atomic masses due to the water molecules by the sum of all the atomic masses in the hydrate, and multiply the result by 100. Complete the table. | BaCl2 | BaCl2•H2O | BaCl2•2H2O | BaCl•3H2O | Sum of atomic masses (BaCl2) | 208.23 | 208.23 | 208.23 | 208.23 | Sum of atomic masses (nH2O) | 0 | 18.02 | 36.04 | 54.06 | Sum of atomic masses (hydrate) | 208.23 | 226.25 | 244.27 | 262.29 | Percent water in hydrate (theoretical) | 0% | 7.96% | 14.75% | 20.61% | In this lab we used a Balance, centigram
This reaction can be summed up using the following formula: 5Fe2++8H++MnO4- →5Fe3++Mn2++4H2O After standardization, the potassium permanganate solution is then titrated with 3 different magnesium oxalate solutions. To find the concentration of the C2O42- the balanced net ionic redox reaction formula is used: 5C2O42-+16H++2MnO4- →10CO2+2Mn2++8H2O It is important to note the addition of sulfuric acid (9M H2SO4) in performing this experiment because of the following reasons: 1) Sulfuric acid keeps the iron (II) from air oxidizing into iron (III) 2) Sulfuric acid keeps the iron (II) from hydrolyzing into Fe(OH)2 3) Sulfuric
ABSTRACT Isopropyltoluene isomers were synthesized through the friedel-crafts alkylation of toluene with 2-chloropropane in the presence of aluminum chloride as a catalyst. Through extraction of the distillate with water and 5% NaHCO3, followed by a fractional vacuum distillation, the desired aromatic organic compound was isolated. Infrared Spectroscopy and Gas Chromatography were used to analyze the composition, purity and to confirm the identity of the prepared product. The sample weighed approximately 2.66g, which reflected a low yield at 47%. However, from the GC the area % (also known as percent purity) was 91.8%, which indicates that a very pure product was obtained.
How do you go from calculated/measured values to accomplishing stated purpose? (4 pts) The purpose of this lab is to determine the exact concentration of an unknown acetic acid solution. Titrations for two different reactions will be performed. Controlled volumes of one reagent are added to a flask containing the other reagent until the equivalence point of the reaction is reached, one between sodium hydroxide (NaOH) and potassium hydrogen phthalate (KHP) and the other between NaOH and acetic acid (CH3COOH). NaOH (aq) + KHP (aq) —› Na+ (aq) + K + (aq) + P2- (aq) + H2O (l) NaOH (aq) + CH3COOH (aq) —› Na+ (aq) + CH3COO- (aq) + H2O (l) The titration of NaOH with KHP will identify the concentration of the NaOH provided.