The purpose of this lab is to focus on how to make zinc iodide in a different way using compounds instead of elements, which are barium iodide and zinc sulfate. We will see if the reaction between these two compounds will occur and make a prediction by writing a chemical equation. The procedures for this lab are to place a small test tube inside a 50mL beaker and weigh it. Then, using a spatula, add 0.45±0.03 g of zinc sulfate heptahydrate into the small test tube and record the mass. After that, dissolve the sample in 2 mL of deionized water and shake the test tube for 1 to 1 ½ minutes to dissolve the solid.
We used 1g of Na2CO3 -Sodium Carbonate. This would allow for the full precipitate to form. 4) Procedure: Refer to CHE 111 lab manual, experiment Stoichiometry of a Precipitation Reaction on page #104 5) Data / results. We used 1g of Na2CO3 -Sodium Carbonate in combination with 1g CaCl2·2 H2O-Calcium Chloride, Dihydrate to form the precipitate reaction. Na2CO3 aq + CaCl2*2H2O aq = CaCO3 s + 2 NaCl aq + 2 H2O aq Molar Mass: Ca = 40.08 Cl2 = (35.45) x 2 = 70.9 2H2O = (18.02) x 2 = 36.04 40.08 + 70.90 + 36.04 = 147.02 g/mol CaCl2*2H2O Theoretical yield: 1g CaCl•2H2O x 1 mol CaCl•2H2O x 1 mol CaCO3 x 100.09g CaCO3 = 0.68 g CaCO3 147.02g CaCl•2H2O 1 mol CaCl•2H2O 1 mol CaCO3 Mass of weighing dish = 0.6g Mass of filter paper =
Write a hypothesis on what you think will happen when water is added. 3. Fill the test tube with two thirds of water and record the results. Copper (II) Sulphate Solution and Iron Nail 1. Record physical properties of the copper (II) sulphate
The following data were obtained when a sample of barium chloride hydrate was analyzed as described in the Procedure section. Calculate (a) the mass of the hydrate, (b) the mass of water lost during heating, and (c) the percent water in the hydrate. Mass of empty test tube 18.42 g Mass of test tube and hydrate (before heating) 20.75 g Mass of test tube and anhydrous salt (after heating) 20.41 g. Mass of the Hydrate is 2.33g. Loss (H2O) is 0.34g. Percent H2O in Hydrate is equal 0.34/2.33=14.6% 3.
The absorption spectrum is measured using a spectrophotometer and the data is graphed in Excel. The peak of the line is used to find Vmax of Fe2+. Vmax is used to find the moles of Fe2+ and ligand. The unknown n is a ratio of moles ligand divided by moles Fe2+. Results and Discussion For the first part of the experiment (Part A), five different 100 mL volumetric flasks were each filled with 1,2,3,4 and 5 mL of iron (II) solution.
Lab # 4 : The Redox Arena II Procedural Summary There will be three different sized test tubes that will be used in this experiment, a boiling tube, a large and small test tube. The boiling tube will be labeled “R” for “reactants”. A scale with a weighing paper will be tared before adding 2 grams of granular zinc (Zn), record the mass, and then move the zinc to the boiling (R) tube. Weigh out 2 grams of iodine crystals, record it, and this will be added to the R tube, with the zinc. The R tube will then be put in a large beaker.
0.00079 moles EDTA4- c. 0.00079 moles ZnI2 d. 0.0517 grams of ZnI2 are in the sample e. 0.0517/0.237= 21.8% f. Error Is 6.34% Lab Report: Part 1: In this lab we used the following supplies: * Zinc Iodide * Na2H2EDTA(s) * Calmagite indicator solution * pH 10 buffer solution * 6M Acetic Acid * Unknown Zinc Compound The main purpose for this part of the lab was to determine the amount of zinc ion in a sample of ZnI2 by titration. The two types of zinc: * Zinc iodide made by zinc and iodine * Commercially purchased zinc iodide (the
Stoichiometry is a section of chemistry that involves using the relationships between reactants or products in a chemical reaction to determine the desired quantitive data. 4. Using the balanced chemical reaction between Sodium carbonate and Calcium Carbonate given in page 92 of your lab manual (first paragraph of procedure), find the mass of Sodium Carbonate (in grams) needed in reaction? Na2CO3(aq)+CaCl22H20(aq)-CaCO3(s)+2NaCl(aq)+2H2O Date:_____3/30/2015____________ Name______Chloe Flake______________ 1. Title: 1pt Stoichiometry Of A Precipitation Reaction 2.
Part C: Density of Sodium Chloride (NaCl) Solution, a sample of NaCl was obtained and measured using a 100mL beaker and a 10mL pipet to determine the concentration of the solution. In order to obtain the appropriate result, a calibration graph and density measurement was used to determine the concentration of the sodium chloride solution. In conclusion, based on the water temperature of 21.8°C in part A’s graduated cylinder experiment obtained, it was determined that the average density was .0973g/mL with a percentage error of 2.5%. When graphed the measurement was equal to Y=0.988x. Part B: The graduated pipet’s average density at 22.3 °C was determined to be 0.9785g/mL with a percentage error of 1.89% shows the graduated pipet to be more accurate and precise.
Procedure: Throughout this lab we were finding the physical properties of substance B. We found the boiling point, freezing point, density and solubility in water, hexane and Alcohol. We started by finding the boiling point