Diels Alder Lab

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CHE 326 Experiment 4 The Grignard Reaction I. PRE-LAB (please complete before coming to lab, should be typed, 1 page limit) [pic] A. Table of Reagents (fill in all the blanks as described in the instructions). |Compound |Mol. Weight | |amount |m p | | | | | |mmol |(in g or mL) |(deg C) |density |Ref. | |bromobenzene |157.01 |4.00 |0.63g |-31 |1.49 |1 | |magnesium powder |24.305 |4.00 |0.097g |649-651 |1.74 |2 | |ethyl ether |74.12 |2.89 |3ml |-116 |.714 |3 | |benzophenone |182.0694 |3.8 | |49 |1.11 |4 | |triphenylmethanol |260.32 | | |164.2 |1.199 |5 | |5% HCl (aq.) |36.46 | |2ml |-74 |1.0-1.2 |6 | B. References (provide references for the information you've given in the table of reagents) 1. http://fscimage.fishersci.com/msds/03420.htm 2. http://WWW.jtbaker.com/msds/englishhtml/m0088.htm 3. http://fscimage.fishersci.com/msds/90868.htm 4. http://fscimage.fishersci.com/msds/02740.htm 5. http://fscimage.fishersci.com/msds/45870.htm 6. http://fscimage.fishersci.com/msds/95551.htm C. Safety (are any of the reagents used toxic or hazardous? Briefly explain here) 1. Bromobenzene causes skin

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