It displays the peak area on the Y axis and the concentration on the X axis. 9 Conclusion: The main purpose of this lab was to find the main ingredients in an Excedrin tablet as well as how much of each ingredient is in the tablet. Two different techniques were used to help develop the ingredients. The two techniques used were extraction and HPLC. It was concluded that Excedrin tablets consist of acetaminophen, aspirin, and caffeine.
Separation of the components of Extra-Strength Excedrin I: Acid-Base extraction Introduction The purpose of this experiment is to analyze the purity of Extra-Strength Excedrin® by utilizing thin-layer chromatography and determine the percent recoveries of its components. Three active ingredients will be extracted and collected from two tablets of Extra-Strength Excedrin® by utilizing acid-base extraction method. Three active ingredients of Extra-Strength Excedrin® are acetylsalicylic acid(aspirin), acetaminophen and caffeine, and their structures are: In addition, there is a binding material, which binds other three components together. These compounds can be separated by acid-base extraction because of their different acidities. A binding material can be separated by dissolving the tablet in ether since three active ingredients are soluble.
Quality Control for the Athenium Baking Soda Company A Self-Directed Experiment 16 April 2012 INTRODUCTION The Athenium Baking Soda Company has begun producing baking soda (sodium bicarbonate, or sodium hydrogen carbonate). NH4HCO3 + NaCl ==> NaHCO3 + NH4Cl Due to the high concentration of the brine solution that is used to generate the product, contaminants are often present in the finished product as chloride compounds. The contaminants may be detected when the finished baking soda product is dried and filtered. PURPOSE: In this experiment, we will be employing quality control by analyzing the composition and purity of the contaminated baking soda samples. To perform this experiment, we will utilize emission spectra, titrations, and thermal gravimetric analysis, using knowledge from Experiments 10, 4, Titrations of Na2CO3 and NAHCO3 by HCl (hydrochloric acid) will be performed to determine the concentration of HCl, as well as the number of moles of HCl present within the sample of baking soda.
Results Sheet, Experiment 13 Brand of Vinegar used:________________ Acetic Acid % from bottle label_____________ | Initial NaOH Reading(estimate to 0.1 mL) | Final NaOH Reading(estimate to 0.1 mL) | Volume NaOH used(Final – Initial) | Trial 1 | 9.5 | 1.3 | 8.2 | Trial 2 | 9.6 | 1.4 | 8.2 | Trial 3 | 9.7 | 1.4 | 8.3 | Average Volume of NaOH used | 8.2 | Calculations: Normality of the acetic acid: .82 Mass of acetic acid: 49.2 % acetic acid (divide the grams, above, by the volume you used to get g/L): 4.92 Answer questions A-G in the lab manual: A. What is the average % acetic acid in your vinegar sample? Standard vinegar is 5% acetic acid. How does your result compare with the standard? The average was 4.92 which is pretty close comparably to the standard.
EXPERIMENT: TECH 0704, Distillation, macroscale technique only, simple and fractional: Substitute a mixture of 25 mL ethanol and 25 mL water for the toluene/cyclohexane mixture. Record the temperature at 2 mL intervals of distillate. Use glass beads to pack the fractionating column. Construct a graph of temperature vs volume for each distillation in your lab notebook. Compare the efficiencies of the two distillation methods in your lab notebook.
Then you put the remaining liquid (neutral component mixture) through the suction filtration funnel to isolate the crystals. After 10-15 minutes, the crystals will be dry and you can weigh them and find their melting point. How is the neutral component of your 3-compound mixture isolated from the final methylene chloride solution? 16 of 22 4/16/12 9:15 PM StudyBlue Flashcard Printing of Lab Final 2211L UGA http://www.studyblue.com/servlet/printFlashcardDeck?deckId=... Name the four active ingredients that we will be testing for in the TLC of Analgesics lab: Ibuprophen Caffeine Acetaminophen Acetylsalicylic acid What solvent system will you be using to dissolve the common analgesics (power) in preparation for TLC spotting? Methylene chloride: ethanol (1:1 solution) What solvent system will you be using to "develop" your TLC plates in the TLC of Analgesics lab?
Determination of the percentage purity of aspirin Introduction The aim of this experiment is to determine the percentage purity of 2-ethanoyl-hydrobenzoic acid (acetylsalicylic acid) in aspirin tablets. A known amount of standard sodium hydroxide solution is used in excess to hydrolyze a known mass of aspirin tablets: CH3COOC6H4COOH(s) + NaOH(aq) → C9H7O4Na(s) + H2O(l) The unused sodium hydroxide which remains is then titrated with standard nitric acid solution of 1 mol. NaOH(aq) + HCl(aq) → NaNO3(s) + H2O(l) The amount of alkali required for the hydrolysis can now be calculated and from the above equation, the amount of moles of acetylsalicylic acid which has been hydrolyzed can be found. Research question | Independent variablesnumber
1) Jeffrey Cox CHE111-DL01 Lab number 10 Stoichiometry of a Precipitation Reaction 2) Purpose/ Intro. In this lab we will be able to calculate the actual, theoretical, and percent yield of the product from a precipitation reaction. We will thusly learn the concepts of solubility and the formation of a precipitate. A precipitate reaction is a reaction in which soluble ions in separate solutions are mixed together to form an insoluble compound that settles out of the combined solution as a solid. The solid then is the insoluble compound, called a precipitate.
Experiment and Observation: Please note that this procedure was adapted from the “Anions, Cations, and Ionic Reactions” LabPaq Lab manual (Hands-On Labs Version 42-0304-82-00-01, 2015) Please reference this manual for further information on the lab experiments. The first experiment was to perform a qualitative anion test. This was done by observation of chemical reactions and recording the results in Data Table 1. Using the information from the reactions we were able to identify unknown substances and recorded the results in Data Table 1. Data Table 1: Anion Confirmation Tests Chemical | Anion | Addition of AgNO3 | Addition of HCl | NaBr | Bromide | Cloudy white thin solution | Clear with sedimentation | Na2CO3 | Carbonate | Clear with white sedimentation | Bubbles, sedimentation combined to one formation | NaCl | Chloride | Milky white, white sedimentation | No visible change | Nal | Iodide | Pale green cloudy, sedimentation | Sedimentation dispersed to smaller pieces, solution clears in color | Na2SO4 | Sulfate | No visible changes noted | Milky white | Na2S | Sulfide | Clear with amber sedimentation | No visible Change noted | Unknown #103 | CarbonateNa2CO3 | Cloudy white thin solution | Bubbles, Sedimentation combined to one
Lab 12 Experiment 12: Reactions of Amines Aim: 1) To investigate and to determine the chemical properties and chemical reactions of Amines 2) To observe the reactions of Amines Procedure: Refer to the Laboratory Manual of CHM152 page 72 to 74 Result: A. Solubility Compound | Butylamine | Diethylamine | Solubility | Very soluble | Not soluble | B. Salt Formation Solubility of dibutylamine in water: Not soluble Solubility of dibutylamine in acid: Soluble, white fume is produced Result of making the solution alkaline: Cloudy solution is produced C. Reaction with Nitrous Acid Compound | Observations | Butylamine | Bubble gas | Aniline | Yellow solid | N-Metylaniline | Yellow oil opaque green solution | Conclusion: Amines show various chemical properties and chemical reactions when tested with different reagents. Discussion: 1. Do not transfer any of the liquids from the reagent bottles to the beakers placed beside the bottles (the beakers are there to contain Pasteur pipettes). Transfer the liquid directly from the bottle to your test tube.