The aspirator was turned to medium high, and then the copper was poured onto wetted filter paper. Using distilled water to remove all copper from the beaker. Once completely on filter paper 6mL of acetone was added to the copper to help dry it out. The filter paper was then removed and set down to dry completely. Once dry the filter paper was weighed with the copper on it and subtracted from the original weight to see the amount of copper left after
The second experiment, procedure 1, combined [Co(NH3)5 (H2O)]Cl2 (0.0060M, 1.52g) and (25mL) of distilled water to an 125mL Erlenmeyer flask. The flask was gently heated (dial 5-6) and stirred until all the compound was dissolved. The heated solution was then vacuum filtered through a fritted funnel and the filtrate was cooled in an ice bath until the
Gravimetric Determination of Sulfate Purpose The purpose of this lab is to determine the percentage of sulfate in the hydrate by precipitating the sulfate as barium sulfate. Materials Filler paper Sodium sulfate Graduated cylinder Bunsen burner Watch glass Beakers (250 mL, 400 mL) Rubber bulb Graduated pipette Beaker tongs Funnel Filter Paper Sodium Sulfate Drying oven Wash bottle Stirring rod Silver nitrate Hydrochloric acid Distilled water Small test tube Procedures First, .4861 grams of sodium sulfate was placed into a clean 400mL beaker. Exactly 200mL of water and 1mL of HCl was added to the same beaker. A watch glass was placed on the beaker and the solution was heated using the Bunsen burner to a gentle boil. The watch glass was removed with the beaker tongs.
In another flask 50-mL of ice water was deposited with three-drop phenolphthalein. Using a volumetric pipet 50-mL of the 1-bromopropane was added into the empty flask in the bath. By the same method 50-mL of potassium hydroxide was delivered to the same flask while swirling the contents and remaining in the water bath. A 10-mL aliquot was immediately removed from the mixture and added to the ice water containing the phenolphthalein. When the pipet was half emptied into the ice water a timer was started.
Procedure 1. Begin to prepare an EDTA solution. Weigh out 3.62-3.64 g of NaH2EDTA and record exact mass. Add the weighed amount to a 250 ml volumetric funnel carefully using a funnel Wash the funnel with water to ensure all of the solid is delivered to the flask Add 100-200 ml of water and mix. Enough water should be added so that the flask is full to the 250 ml mark Tightly wrap the top of the flask with a Parafilm when finished 2.
Cool the beaker in ice water for 10 min, with stirring, and collect the solid by vacuum filtration on a small Hirsch funnel. Rinse with three small portions of water, by breaking the vacuum, adding just enough water to cover the solid, and reapplying the vacuum as before. Filtration of the fine crystals is slow. Using too much rinse water will slow the process considerably. Allow the solid to dry at least overnight, weigh it, take a MP, and calculate the % yield.
Allow the mixture to cool for a few minutes then filter it, using either gravity or vacuum filtration. (We shall be using vacuum filtration.) Wash the residue in the funnel once with a little water and collect all the filtrate. 4. Pour all the filtrate and washings into a 250cm3 volumetric flask.
5) Swirled the solution until the NaEDTA (s) dissolved entirely. 6) After dissolving the solid, deionized water was added to the volumetric flask to make 250mL of EDTA solution. 7) This solution (from Step 6) was then transferred to a clean 250 mL Erlenmeyer flask and placed inside the desk for safe keeping; using a cork wrapped tightly in Parafilm. The disassociation of NaEDTA in water is expressed by the following equation: Na2H2EDTA (s) + H2O (l) yields EDTA4- (aq) + 2Na+(aq) + 2H+(aq) Na2H2EDTA (s) has a molar mass of 372.24 g/mol. Procedure - Reacting EDTA with your Zinc ion in Zinc Iodine Purpose; The
Using a Buchner funnel, a hose, and a suction flask we created a vacuum filtrator which we used to help remove the remaining liquid on the copper so that we may make a more precise measurement of the mass of the remaining copper. Our final mass of copper was .7951 grams. Results and Discussion: Initial Mass of Cu: .25 grams When we mixed the 5 ml of 6 molar HNO3 the copper had disappeared, indicating it had been used in the reaction. The copper had undergone a single replacement reaction and a decomposition reaction. Initial equation: Cu(s) + HNO3(aq) -> Cu(NO3)2(aq) + NO2(g) +H2O(l) Balanced: Cu(s) + 4HNO3(aq) -> Cu(NO3)2(aq) + 2NO2(g) + 2H2O(l) The copper had replaced the Hydrogen in the HNO3 and the NO3 had also broken down into NO2 and O2- allowing the H+ to bond with it and create
Gently stir the resulting mixture for 30-60 seconds. * Step 4 –Place a suitable filter (cloth, filter paper or a fine sieve) over an empty glass, and secure it with the rubber band. Pour the mixture into the filter. If the mixture is too thick, stir in more of the extraction solution. Leave to filter for about 10 minutes.