Fill the burette with 0.005mol dm-3 potassium manganate(VII) solution. 6. Pour some of the thyme extract solution into a 250cm3 plastic beaker. 7. Using a measuring cylinder, add 50cm3 of 1.0mol dm-3 sulphuric(VI) acid to the thyme extract in the conical flask.
The solution was stirred when the NaOH was added. The solution was turned blue. Third, the solution was heated until the color changed from blue to clear. The solution was stirred to prevent “bumbing.” When the transformation was complete, the beaker was taken off the burner and the precipitate was allowed to settle. The supernatant liquid was then decanted.
After that, dissolve the sample in 2 mL of deionized water and shake the test tube for 1 to 1 ½ minutes to dissolve the solid. Place another dry test tube in a 50mL beaker and weigh it. Find a bottle of barium iodide and record the name and molar mass. Then, weight out either anhydrous barium iodide or barium iodide dehydrate into this test tube and dissolve is it in 2 mL of deionized water. Pour the contents of one of the test tubes into the other and a reaction should occur and you should see a white precipitate of barium sulfate form.
Part A: Spectroscopy 1. 0.05g of Iron(III) Nitrate in a 50-ml beaker. Add 17 mL of distilled water to the beaker and mix with a stir rod until the solid is completely dissolved. 2. Obtain another 50-mL beaker and add 0.05g of Chromium(III) Nitrate to the beaker.
AP Chemistry P2 Experiment 2: Formula of a Hydrate 9/24/2013 Purpose: Calculate the percent composition of water in a hydrate and determine the empirical formula of the hydrate. Procedure: 1) Set up ring stand with ring clamp, clay triangle, crucible with lid, and burner. Adjust the height of the ring stand. 2) Dehydrating Procedures: 3. Measure approximately 1 g of Copper(II) Sulfate Hydrate into the crucible and crucible and lid.
Begin by adding 1 mL of rubbing alcohol to test tube and attach a thermometer to it. b. Place assembly in water bath and begin to heat beaker c. As isopropyl alcohol begins to boil, bubbles begin flowing from the capillary tube d. While temperature is decreasing, record the temp. when the last air bubble comes out of the capillary tube. e. Let assembly cool down and repeat process two more times.
Abstract The focus of this experiment was to analyze the kinetics of a nucleophilic substitution. A mixture of 0.3622-M 1-bromopropane and 0.3622-M potassium hydroxide in an 90:10 ethanol/water solvent provided the reactants for a SN2 reaction to occur in a temperature controlled bath at 50.0˚C. The disappearing reactant was found by titrating timed aliquots during the reaction and then measuring the concentration of hydroxide. The k-value was found to be 0.0202 M-1Min-1. Using the linear form of the Arrhenius equation the activation energy was calculated to be 19.9 kcal/mol.
9) The number of moles of H2CO3 in the reaction NaHCO3 + C2H4O2 NaC2H3O2 + H2CO3 is also the number of moles of NaHCO3. 10) Calculate the number of grams of sodium bicarbonate by multiplying the number of moles of sodium bicarbonate by its molar mass. OBSERVATIONS BEFORE REACTION Total Mass: 165.93 g Total Mass: 165.93 g Mass: Alka Seltzer Tablet: 3.82 g Beaker + Vinegar: 162.11 g Temperature: 20.9 °C DURING REACTION Observations: Alka Seltzer is fizzing and dissolving into the vinegar Gas is being released as bubbles form; it’s carbon dioxide Looks like a nice glass of frothy beer AFTER REACTION Observations:
Experiment 5: Preparation of Cyclohexene- Acid Catalyzed Elimination of Cyclohexanol Ball State University Organic Chemistry Lab 231 (Sec. 5) Dr. Bock/Daniel Miller Tiffany Raber 5 November 2012 Purpose: To prepare an alkene by an elimination reaction of an alcohol in the presence of sulfuric acid as a catalyst to produce a successful yield and desired results for the purity of the alkene. Introduction: The dehydration of an alcohol such as cyclohexanol is a useful technique for generating alkenes. The success of this reaction relies on a dehydration, such as the presence of a strong acid (sulfuric acid). Because this reaction is reversible, a fractional distillation is necessary to produce cyclohexene, water, and some impurities and a simple distillation is followed to further purify the product.
The flasks were thoroughly cleaned with distilled water. 3. Samples of the Ammonium Persulfate ((NH4)2S2O8), Potassium Iodide (KI), Ammonium Sulfate ((NH4)2S2O4), Potassium Nitrate (KNO3), Sodium Thiosulfate (Na2S2O3), and Starch were placed in separate Erlenmeyer flasks. 4. Each flask was labeled according to its content (i.e.