I then poured the mixture on to a solid white piece of paper. I then used a magnet wrapped in clear plastic bag to separate the iron from the mixture. I weighed the iron and calculated and recorded the mass in table 1. I put the remaining mixture in a beaker with 50 mL of distilled water and heated to a boil and removed, then poured the liquid from the beaker into a paper cup. I then added 15 mL of distilled water and heated to a boil and removed, then poured the liquid from the beaker into the same paper cup that held the previous liquid.
Second, methyl benzoate is added to form a new carbon-carbon sigma bond. The intermediate magnesium alkoxide will then be hydrolyzed to form tertiary alcohol product. Experimental Procedure: Part A: Preparing the Grignard reagent • I placed 1.98 grams of magnesium turnings into a cleaned 250mL round-bottom flask and then attached the calcium chloride drying tube into the round-bottom flask • Then, I placed this flask onto a heating mantel and adjust the controller to setting ‘6’. This flask is heated until it was too hot to touch. • After the flask was heated, I removed it from the heating mantel and allowed it to cool to room temperature.
Purpose: The purpose of this lab is to verify Hess’s Law of Additivity of Reaction Enthalpies Chemical Reaction/Physical Reaction: 1.) Na(aq) + OH(aq) -> NaOH(s) 2.) NaOH + HC2H3O2(aq) -> H2O(l) + Na(aq) + C2H3O2 3.) Na(aq) + OH(aq) + HC2H3O2(aq) -> H2O(l) + Na(aq) + C2H3O2 List of Materials:Digital Thermometer, foamed polystyrene cups (3), 250 mL beaker,Weighing boat or small beaker, Graduated cylinders, 100mL(1), 25 mL(2),sodium hydroxide pellets, sodium hydroxide 2.0M, Acetic acid 1.0M and 2.0M. Safety Considerations: Always have safety goggles covering your eyes, do not inhale the fumes of chemicals used.
8. Placed the remaining mixture, containing sand, benzoic acid and table salt into beaker and added 50mL of distilled water. 9. Set up the beaker stand and burner fuel and heated the beaker of solids and water to near boiling. Stirred the mixture to make sure all soluble material dissolves.
Extraction and Drying: Using a separatory funnel, the cooled filtrate was extracted with 10ml of methylene chloride. After shaking our mixture, we broke and dried our emulsion by slowing passing the lower layer through a cotton ball layered with anhydrous magnesium sulfate. The extraction process was repeated 2 more times for maximum collection of the organic layer. Distillation: The extracts were poured into a 50ml round bottle flask and connected to a simple distillation apparatus. To obtain the caffeine, the methylene chloride was removed from the extract, leaving us with our solid caffeine residue.
Duplicating a Color with Dye Trohimczyk, Brianna; Delgado, Theon Purpose: The purpose of this experiment is to match the color of the control dye with the new color of the dye produced in the test tube. Hypothesis: When two drops of red dye are placed with one drop of yellow dye in a test tube of water, the result will match the color of the controlled dye. Materials: * Four colors of food coloring (red, green, blue, yellow) * Test tubes * Pipets Procedure: 1. Place water into a plastic cup 2. Use the pipet to place 10ml of water into an empty test tube 3.
.40g of NaH_2PO_4, and .40g of Na_2HPO_4 was measured into a 150 mL beaker. 50mL of distilled water was then measured in to a graduated cylinder and added to the 150ml solution of NaH_2PO_4 and Na_2HPO_4. 20 drops of the .04% Bromothymol blue solution was then also added to the buffer solution. After adding the 20 drops the tint of the liquid changed to a light green. The Vernier pH probe was calibrated and used to determine the pH of the phosphate buffer solution which was 6.81.
Hydrochloric acid was then added to the solution until the bubbles stopped in order to completely get rid of all of the zinc. Next, we used vacuum filtration to filter the copper out of the solution. We drizzled alcohol and acetone over the copper to help it dry faster. Once it appeared dry, we weighed the copper and filter paper. When we subtracted the mass of the filter paper, the mass came out to 1.312g.
Lab #3/Limiting Reagents Abstract The purpose of this laboratory experiment was to determine whether an unknown compound was sodium carbonate or sodium hydrogen carbonate by reacting a sample of it with hydrochloric acid and comparing the resulting yield of NaCl to the calculated values. The mass of an evaporating dish was taken at the start of the experiment. Then the unknown carbonate A was added in the amount of approximately one gram. The dish was weighed once more to find the definite mass of the unknown carbonate. Then, by means of a dropper bottle and stirring rod, hydrochloric acid was added until all of the unknown carbonate appeared to have reacted.
The mixture was decanted again in to the same beaker. Next, we added boiling chips to the liquid and evaporated the solvent over the hot plates under the hood. After the solvent was evaporated and the flask was cooled, we used a spatula to remove a small amount of the crude product and took its melting point. We determined the melting point range of the sample to be 43.0-46.0 degrees Celcius.The crude product was yellow colored when it was warm and orange in color when cooled and sticky. We then recrystallized our sample using 5 ml of warm acetone that was heated on a hot plate under a hood.