Synthesis Of Alum

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Experiment #4: Muddy Waters Chemistry 1001 Taylor Ward Tuesday P.M. Rm. 106 T.A.: Kevin Monday October 24th, 2011 Abstract: For the first part of lab 4 we synthesized potassium aluminium sulfate dodecahydrate (KAl(SO4)2 12H2O), after the synthesis process was completed we used the product to try and clear a beaker of muddy water. We used aluminium that was dissolved into solution and the addition of an acid to create the final alum crystals; with these processes we were able to identify the percent yield of the alum. We could also determine the efficiency of our alum at clearing the beaker of muddy water. Introduction: The purpose of the experiment is to see the chemical process of aluminium foil, potassium hydroxide (KOH), and sulphuric acid (H2SO4) to have alum (KAl(SO4)2 12H2O) crystallize as a product. The compound is used widely for the treatment of wastewater in plants, water purification, the preparation of some food products, and dyeing of fabrics. The method used during this experiment was suction filtration; it uses a vacuum caused by water to filter out any impurities and also to collect any product that is created during the experiment. The equipment used during this experiment was a Buchner funnel that is attached to a filter flask with the use of a rubber ring to ensure that suction can occur. Various chemical reactions that occured from mixing the scrap aluminium pieces and potassium hydroxide to get the aluminium into solution. Then the addition of the sulfuric acid to form the valuable compound of alum, the reason we preformed these reactions was to see our ability to create a useful compound as well as see its effectiveness at clearing water that is full of soil and silt. The background of this experiment is that Aluminium is a “reactive metal” but with a layer of aluminium oxide that surrounds the surface acids take a much
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