Juliana Park Mayumi Tamada CHEM 111B LAB/ M-F 1-4PM 15 August 2012 Spectroscopy Lab Introduction In this lab, the molar absorptivity of the complex FeLn2+ will be determined by using the absorbance of the complex and its concentration. The absorbance will be found by using a spectrophotometer. For the next part of the lab, the formula of the complex will be determined by also using the volume of ligand and the absorbance again. Experimental There are two different parts to the experiement. In the first part, five 100 mL flasks of 5 mL ligand solution, 5 mL 2 M sodium acetate, 4 mL 3 M NH2OH, and 1-5 mL Fe2+ solution are diluted with water.
The purpose of this lab is to focus on how to make zinc iodide in a different way using compounds instead of elements, which are barium iodide and zinc sulfate. We will see if the reaction between these two compounds will occur and make a prediction by writing a chemical equation. The procedures for this lab are to place a small test tube inside a 50mL beaker and weigh it. Then, using a spatula, add 0.45±0.03 g of zinc sulfate heptahydrate into the small test tube and record the mass. After that, dissolve the sample in 2 mL of deionized water and shake the test tube for 1 to 1 ½ minutes to dissolve the solid.
pyridinium hydrobromide perbromide type of stationary phase column length column temperature rate flow of the carrier gas List the 4 general factors that affect the separation obtained on a gas chromatograph What specific technique is used to collect/isolate your purified unknown compound at the end of the recrystallization experiment? suction filtration 14 of 22 4/16/12 9:15 PM StudyBlue Flashcard Printing of Lab Final 2211L UGA
Experiment: Ionic Reactions Derrick Davis Lab partner: None Location: My house Date Performed 19 Mar 15; 0800 CHE111-CO2 Abstract: The goal of this experiment was to work with Ionic substances. The purpose of this experiment was to study and apply the nature of ionic reactions, write balanced equations, and gain a detailed view of the results of the reactions. In this lab we were able to identify some of the characteristics of anions and cations. I was a able to successfully perform the flame test to identify cations as well as identifications of the anion reactions of an ionic compound. Experiment and Observation: Please note that this procedure was adapted from the “Anions, Cations, and Ionic Reactions” LabPaq Lab manual (Hands-On Labs Version 42-0304-82-00-01, 2015) Please reference this manual for further information on the lab experiments.
Aim To compare the reactivity of various metals by observing their reaction with hydrochloric acid Hypothesis That the all the metals will produce foam and a pop. Variables Independent – Magnesium, Aluminium, Zinc, Copper Dependent – Detergent, Hydrochloric Acid Controlled – Size of the metals, amount of detergent and hydrochloric acid Materials 2 M hydrochloric acid Detergent 10 x test tubes and test tube rack and 5 rubber stoppers 0.5 cm pieces of magnesium, aluminium, zinc and copper 2 cm pieces of magnesium, aluminium, zinc and copper Steel wool Ruler Timer Bench mat Matches and birthday candle Marking pen Safety Remember to wear safety glasses and protective gloves when you do this experiment. 2 M HCl is corrosive. Wash with plenty of water should you get any on your skin or in your eyes. Method Part 1 1 Clean the surface of the 0.5cm piece of magnesium with a piece of steel wool 2 Place the magnesium into a test tube 3 Add three drops of detergent to the test tube 4 Add 2 cm of hydrochloric acid to the test tube.
0.00079 moles EDTA4- c. 0.00079 moles ZnI2 d. 0.0517 grams of ZnI2 are in the sample e. 0.0517/0.237= 21.8% f. Error Is 6.34% Lab Report: Part 1: In this lab we used the following supplies: * Zinc Iodide * Na2H2EDTA(s) * Calmagite indicator solution * pH 10 buffer solution * 6M Acetic Acid * Unknown Zinc Compound The main purpose for this part of the lab was to determine the amount of zinc ion in a sample of ZnI2 by titration. The two types of zinc: * Zinc iodide made by zinc and iodine * Commercially purchased zinc iodide (the
0.05mol/6M=8.3*10-3 L=8.3mL stock solution c. 100mL-8.3mL=91.7mLwater Add 91.7 water to 6M stock solution to prepare 0.5M acetic acid. Exercise 8: a. 42.35 - 0.55 = 41.8 mL b. The moles of EDTA4- : 0.0189M*(41.8*10-3)L=7.9*10-4mol c. Zn2+(aq)+EDTA4-(aq)—Zn(EDTA)2-(aq) The ratio Zn2+ and EDTA4- is 1:1 The moles of Zn2+= the moles of EDTA4-=7.9*10-4mol d. 7.9*10-4mol*65.39g/mol=0.0517g Zn e.
Prelaboratory preparation: Read pages 1 – 30 and 45 – 54 of the lab text. You may disregard the microscale distillation procedures of TECH 0704. Answer in your laboratory notebook the Safety Quiz on pages 11 – 12 and the Prelab Questions 1, 2a, 2b, 3 -5, pp. 67 - 68. EXPERIMENT: TECH 0704, Distillation, macroscale technique only, simple and fractional: Substitute a mixture of 25 mL ethanol and 25 mL water for the toluene/cyclohexane mixture.
For example, if you mix aqueous solutions of AgNO3 and NaCl, there are two new combinations of ions possible. The silver nitrate solution contains Ag+(aq) and NO3-(aq). The sodium chloride contains Na+(aq) and Cl-(aq). Possible new combinations of these ions are AgCl and NaNO3. Note: these formulas would have been written in the upper right hand corner of each box before beginning the lab.
Experiment 6: Physical & Chemical Properties Title and Identifiers: Heating of chemical properties 01/23/15 Purpose / Objective: • To investigate the chemical properties of pure chemical substances • To investigate the physical properties of pure chemical substances Procedural Outline: • Matches • Beaker, 100 mL, glass • Burner-fuel • Goggles-Safety • Stirring rod - Glass • Test Tube(5), 13 x 100 mm in Bubble Bag • Test-tube-clamp-holder • Test-tube-cleaning-brush • Well-Plate-24 • Well-Plate-96 • Litmus Paper, Blue • Litmus paper, Red • Copper (II) Carbonate in Vial, 1/2 Full • Copper (II) Nitrate Crystals in Vial • Copper Metal