Measure and record the mass of the test tube and metal. 5. Place the test tube containing the metal into the beaker of water and continue heating (10 min). Leave the test tube in the boiling water bath while you complete steps 6 and 7. 6.
Materials: 250mL Beaker Test Tube Calorimeter Burner, Ring Stand, and Wire Gauze Thermometer Balance Procedure: 1. Prepare an appropriate data table. 2. Fill the 250mL beaker about half full. Place it on the stand and begin heating it to the boiling point (100 degrees Celsius).
7. Attach beaker clamp to retort stand Attach cord to beaker clamp Put light bulb into cord socket Place beaker under retort stand Adjust beaker clamp to position light bulb approximately 5-6cm. above beaker Fill beaker with the predetermined amount of a listed substance Place thermometer in beaker for 1 minute to determine the starting temperature of the substance 8. Remove the thermometer and turn on light bulb for 8 minutes 9. Turn off light and place thermometer in substance for 1 minute in order to determine the ending temperature 10.
Fill a 10 mL graduated cylinder with ≈ 7mL if water c. Fill a 1000 mL beaker with ≈ 750 mL of water d. Invert the graduated cylinder into the beaker. Add water to the beaker to completely submerge cylinder. e. Measure the difference between the height of the water in the graduated cylinder and the height of the water in the beaker. f. g. Record the barometric pressure in mmHg. Heat the water via Bunsen burner to 80°C.
Record the combined weight 4. Determine the weight of the water by subtracting the empty beaker weight (step 1) from the weight of the beaker plus 50 ml of sea water (step 3) 5. Place beaker on hot plate and evaporate most of the water. Record the time and temperature at which the seawater begins to boil. As the water is being evaporated, record the temperature every 2 minutes.
The mass was recorded and transferred to a 50 ml beaker. 4 ml of 6 M HNO3 was added to the beaker containing the copper. For step 2, 10 ml of distilled water was added to the beaker. Then, 6 M NaOH was added to the solution (drop wise), until placing a drop of the solution on red litmus paper turned it blue. For step 3, the solution was heated with a hot plate.
Materials Protective Glasses | Beaker (250ml) | Stirring rod | Filter funnel | Filter paper | Evaporating basin | Bunsen burner | Heat resistant mat | Tripod | Gauze | Sand | Salt | Matches | | | Method After collecting all the materials needed for the experiment, the students were asked to weigh a mixture of sand and salt (5g) into a 250ml beaker. They also weighed the combined weight of the beaker and salt and sand mixture. They then poured 50ml of distilled water into the beaker, making sure to stir well with a stirring rod to dissolve all of the salt. They then weighed a piece of filter paper, folded it into a cone shape that would fit into the filter funnel, pressing it onto the inner walls of the funnel to make sure no sand would be lost in error. (See diagram below) Water was poured through the filter funnel.
Microcalorimetry experiment was performed on Setaram−C80 heat flow calorimeter coupled to a multiport high-vacuum homemade glass manifold. A specific amount of the sample (approx. 500 mg) was taken into a sample cell, reference cell was taken as empty and together they are connected with Pyrex tee. The sample was heated from room temperature to 200°C under vacuum and kept for 2 h, then 3-4 doses of helium gas were introduced into the system to remove any excess residue such as moisture or organic impurity from the system. The system was heated for 4-5 hr under vacuum at 200°C and then cooled down to the temperature (50°C) where we want to perform the adsorption study.
Procedure Preparing of Medium Agar Materials and apparatus * Distilled water * Nutrient agar powder * Autoclave machine * Petri dish * Hot plated * Conical flask Procedure 1. 500 ml of agar solution was prepared by using 500 ml distilled water and 10 g of nutrient agar powder. 2. Both distilled water and nutrient agar powder was poured into conical flask. 3.
Gravimetric Determination of Sulfate Purpose The purpose of this lab is to determine the percentage of sulfate in the hydrate by precipitating the sulfate as barium sulfate. Materials Filler paper Sodium sulfate Graduated cylinder Bunsen burner Watch glass Beakers (250 mL, 400 mL) Rubber bulb Graduated pipette Beaker tongs Funnel Filter Paper Sodium Sulfate Drying oven Wash bottle Stirring rod Silver nitrate Hydrochloric acid Distilled water Small test tube Procedures First, .4861 grams of sodium sulfate was placed into a clean 400mL beaker. Exactly 200mL of water and 1mL of HCl was added to the same beaker. A watch glass was placed on the beaker and the solution was heated using the Bunsen burner to a gentle boil. The watch glass was removed with the beaker tongs.