The buret had used the NaOH thoroughly rinsed three times because at the first titration the NaOH solution was used. About 50Ml the NaOH solution was in a clean beaker and brought it to experiment area. A funnel was used to fill the NaOH into the buret and recorded the initial volume on the buret to the correct number of significant figures. A pipette was used to take 10.00ml HCl into a clean 50mL Erlenmeyer flask. Three drops of phenolphthalein indicator was added into the HCl solution.
4) Ignoring step 3, after step 2, you can take the solution that you have created and pour it into a 100 mL beaker. Once the solution is in the beaker, turn on the conductivity tester and gently place it in the solution (try not to touch the bottom of the beaker). Record the results. 5) Now, take the beaker with the solution already inside and place it on a hot plate. Turn on the hot plate to a medium heat.
When the liquid above the precipitate was clear, the solution was tested for completeness of precipitation when a few drops of BaCl2 solution were added from a pipette. Next, filter paper was place into the funnel and streamed with distilled water. A clean 400mL beaker is placed under the funnel and the precipitate was filtered through. When all the precipitate was filtered and removed from the beaker the residue is washed with distilled water. About 3mL of the wash water is collected in a small test tube.
The Determination of Keq for FeSCN2+ Purpose: To determine the equilibrium constant Procedure: Part I - Preparing the solution 1)Get 10 test tubes 2)Prep the 5 reference solution test tubes. Mix each solutions using a stirring rod. Standard Volume of .200M Fe(NO3)2 Volume of .00020M KSCN solution Reference Solution #1 8.0mL 2.0mL Reference Solution #2 7.0mL 3.0mL Reference Solution #3 6.0mL 4.0mL Reference Solution #4 5.0mL 5.0mL Reference Solution #5 4.0mL 6.0mL 3)Using he burets transfer the appropriate volumes of each reagent to make the test solutions. Sample .0020M Fe(NO3)2 .0020M KSCN Distilled Water Test Solution #6 5.0mL 1.0mL 4.0mL Test Solution #7 5.0mL 2.0mL 3.0mL Test Solution #8 5.0mL 3.0mL 2.0mL Test Solution #9 5.0mL 4.0mL 1.0mL Test Solution #10 5.0mL 5.0mL 0mL 4) Mix each solution using a stirring rod 5)Measure the temperature of one of the solutions and record. Part II - Spectral Analysis 1)Ensure that the instrument has had time to warm up for 15 min.
Then by writing a balanced chemical equation and using the titration formula, Nb+Ma+Va=Na+MbVb , the molarity is able to be determined. Procedure: 1) Using the graduated cylinder add 10.0 mL of water into the Erlenmeyer flask. 2) Add 5.0 mL of HCl into the flask using another graduated cylinder because acid goes into water when mixing them. 3) Add three drops of phenolphthalein indicator into the flask. 4) Swirl the flask in circular movements to mix the substances.
Distilled water Dropper 2x 5 mL measuring cylinders Method Step 1) Pour 5 mL of distilled water into the 5mL measuring cylinder. Then select one of the five alcohols and add 5 drops of each alcohol with the 5 milliliters of water. Step 2) Let the solution sit for one minute to make sure that the result will be clear Step 3) After you carefully observe the beaker with the solution, make sure you wash it thoroughly before using It for the next trial/test. Repeat for all six types of alcohols using the same apparatus every time to make sure the result are as accurate as possible. | Methanol | Pentanol | Ethanol | Propanol | Glycerine | Butanol | Soluble | | | YES | | YES | | Insoluble | | YES | | | | | Partially Soluble | YES | | | YES | | YES | RESULTS Discussion The data together unevenly displays that the alcohols with larger molecules have less solubility in distilled water.
Independent Variables: • The range of pH, between 6-8 pH. Method: 1. Firstly, place the buffer tablets into a test-tube containing 20 ml of water (at room temperature). 2. Once the buffer tablet has dissolved into the water, add 10 ml of starch solution.
The third test will utilize thin layer chromatography to evaluate the purity of the aspirin as well as testing for the presence of leftover salicylic acid or other by products of the reactions. Experimental: Week 1: For the synthesis of the aspirin, 250 mL of water was boiled. 1.5 g. of salicylic acid were poured on a test tube. Then, 3.5 mL of acetic anhydride and four drops of 85% phosphoric acid were added. A cotton ball was placed to prevent vapor escape.
The extraction process is when a solvent, dichloromethane (15mL) is added to the filtrate in a separatory funnel; the mixture is gently swirled together 3 times, and stopcock is released in between to vent the funnel. Dichloromethane (including the emulsion) is then drained from the bottom into a 50mL Erlenmeyer flask. Same extraction process is repeated on the same filtrate and the dichloromethane is, once again, let out to the same 50mL Erlenmeyer flask as before. The combined dichloromethane solution and water (20mL) is poured into a rinsed separatory funnel. Mixture is gently swirled and drained out into an Erlenmeyer flask.