Cylinder was rinsed with distilled water. * * 2. 2.0 ppm standard: 2.00 mL of 10.0 ppm phosphate solution was placed in a 25 mL graduated cylinder and diluted to exactly the 10 mL mark with distilled water then poured into a plastic cup labeled 2. Cylinder was rinsed with distilled water. * 3.
For every 20 drops of solution you will add 0.1g of zinc to the new test tube. Repeat steps 3 and four until the solution is clear. If there ever exists too little of the solution to get enough drops, add up to 1mL of distilled water to the solution. 4. Once the solution is clear, retrieve at least ten drops of the solution and place them in a new test tube.
Materials and Methods Part 1 For the cation elimination test first 10 drops of potassium, iron (III), zinc (II), copper (II), and cobalt (II) were added to 5 centrifuge tubes and the color was recorded. Then for the metal hydroxide test, 6 M NaOH was added drop wise till a precipitate was formed. Each solution except potassium formed a precipitate, so then 10 additional drops of NaOH were added to the remaining solutions. Tubes were cleaned with distilled water and 6 M HCL. Next was the ammonia test 10 drops of each metal solution were added to new centrifuge tubes and 15 M NH4OH was added until the solution changed color or a precipitate was formed.
Sodium Iodide in Acetone: * The Experiment: * Label ten test tubes from1 to 10. * Place 2 mL of a 15% Nal-in-acetone solution in each test tube + 4 drops of one of the following halides to the appropriate test tube: * (1) 2-chlorobutane, (2) 2-bromobutane, (3) 1-chlorobutane, (4) 1-bromobutane, (5) 2-chloro-2-methylpropane (t-butyl chloride), (6) crotyl chloride CH3CH=CHCH2Cl (7) benzyl chloride (a-chlorotoluene), (8) bromobenzene, (9) bromocyclohexane, and (10) bromocyclopentane. * Reaction at Room Temperature: * Shake the test tube2 After adding the halide * Record the times needed for any precipitate or cloudiness to form. * Reaction at Elevated Temperature: * After about 5 minutes, place any test tubes that do not contain a precipitate in a 50°C water bath. * Be careful not to allow the temperature of the water bath to exceed 50°C, because the acetone will evaporate or boil out of the test tube.
The resulting product was [Co(NH3)5Cl]Cl2 and yield was 4.453g (.017 mol, 84.8%) Distilled water (25mL) was added to concentrated ammonia (5mL) in a 125mL Erlenmeyer flask. The reaction was heated and stirred, then [Co(NH3)5Cl]Cl2 (.0060 mol) was added to the solution. The reaction mixture was vacuum filtered, and the filtrate was cooled in an ice bath. 6M HCl was then added until the solution was neutral to litmus. NaNO2 (.0217 mol) was added to the solution and was allowed to react for five minutes.
Procedure: Refer to Chemistry Lab Manual pp. 33-35, 37. Results: The density of the yeast-sugar solution on day 1 was 1.05g/mL. On day 2, the density of the solution had dropped down to 1.00g/mL. We found the mass of our pure alcohol to be 10.23g.
White precipitate shows the presence of chloride (Cl-). Chloride anion equation: HCl(aq) + AgNO3 (aq) → HNO3 (aq) + AgCl(s). The nitrate anion test involves cooling a mixture containing 1 mL of test solution and 3mL 18M H2SO4. 2mL is poured down the inner test tube side and the presence of a brown ring shows nitrate (NO3-) to be present. The carbonate anion test mixes 1 mL of test solution and drops of 6M HCl.
Use 10 mL of the stock and dilute to 1 L with distilled water. This gives a 0.01 M solution. 7. Yeast suspension: Add 1 package of dry yeast to 250 mL of 1% sodium bicarbonate solution. Mix thoroughly and swirl when dispensing.
Materials and Methods Part 1 – Cation Tests Potassium, iron (III), zinc (II), copper (II), and cobalt (II) cation solutions were made subject to two elimination tests involving the addition of sodium hydroxide in one and ammonium hydroxide in the other. Approximately 10 drops of each cation solution were placed in 10 different centrifuge tubes. To begin the sodium hydroxide test, 6M NaOH solution was added to one sample of each cation solution until either a precipitate was formed or until 20 drops were added. An additional 10 drops of 6M NaOH was added to each solution in which a precipitate formed and the solutions were shaken lightly to aid in the mixing of the reaction. To begin the ammonium hydroxide test, 15M NH4OH was added to one sample of each cation solution until the formation of a precipitate was observed, with care not to exceed 20 drops.
Put exactly 5.0 mL of water in the 10.0 mL graduated cylinder. Record this volume in your data table (10.0 mL). Label the first pipet "Acid." To calibrate the pipet, fill it with LIU-2 water. Holding the pipet vertically, add 20 drops of water to the cylinder.