We added anhydrous Sodium Sulfate as a drying agent. To complete, we distilled the cyclohexene and collected the product. Knowing this data, we determined the yield % which is 58.5%. This experiment features the dehydration of cyclohexanol and produce cyclohexene. The acid catalyzed dehydration of cyclohexanol with distillative removal of the resulting cyclohexene from the reaction mixture
Name: ___________________________________ Date: ______________ Practice Test #3 ____ 1. When a precipitation reaction occurs, the ions that do not form the precipitate A) evaporate B) are cations only C) form a second insoluble compound in the solution D) are left dissolved in the solution E) none of these 2. An aqueous solution of potassium chloride is mixed with an aqueous solution of sodium nitrate. The complete ionic equation contains which of the following species (when balanced in standard form)? A) B) C) D) E) ____ 3.
To perform this experiment, we will utilize emission spectra, titrations, and thermal gravimetric analysis, using knowledge from Experiments 10, 4, Titrations of Na2CO3 and NAHCO3 by HCl (hydrochloric acid) will be performed to determine the concentration of HCl, as well as the number of moles of HCl present within the sample of baking soda. As a result, we will be able to determine the molar concentration of HCl by determining its equivalence point (the point on the graph where the exact amount of rectant needed to perform a reaction has been added) from graphical analysis. Na2CO3(aq.) + HCl(aq.) ==> NaHCO3(aq.)
Experiment 5: Preparation of Cyclohexene- Acid Catalyzed Elimination of Cyclohexanol Ball State University Organic Chemistry Lab 231 (Sec. 5) Dr. Bock/Daniel Miller Tiffany Raber 5 November 2012 Purpose: To prepare an alkene by an elimination reaction of an alcohol in the presence of sulfuric acid as a catalyst to produce a successful yield and desired results for the purity of the alkene. Introduction: The dehydration of an alcohol such as cyclohexanol is a useful technique for generating alkenes. The success of this reaction relies on a dehydration, such as the presence of a strong acid (sulfuric acid). Because this reaction is reversible, a fractional distillation is necessary to produce cyclohexene, water, and some impurities and a simple distillation is followed to further purify the product.
n (3) Solutions of aqueous sodium hydroxide and hydrochloric acid react to form water and aqueous sodium chloride. co NaOH(s) → Na+(aq) + OH–(aq) ∆H1 = ? Chemistry with Vernier py In this experiment, you will use a Styrofoam-cup calorimeter to measure the heat released by three reactions. One of the reactions is the same as the combination of the other two reactions. Therefore, according to Hess’s law, the heat of reaction of the one reaction should be equal to the sum of the heats of reaction for the other two.
Manganese dioxide is an inorganic molecule that can achieve this. The catalyst lowers the activation energy of the decomposition which is already noticeable without the addition of a catalyst. In our lab we observed that the Manganse dioxide had no effect on the reaction, however it should have a significant
This product, dibromocholesterol, was washed and debrominated by an elimination reaction using zinc dust. Percent yield and recovery evaluated the efficiency of this synthesis. Melting point and thin layer chromatography (TLC) analysis assessed the purity of commercial cholesterol, dibromocholesterol, and synthesized cholesterol by physical analysis. Chemical tests evaluated the purity of these samples by assessing the presence of specific functional groups. Silver nitrate tested for 2o and 3o alkyl halides expected in dibromocholesterol and sulfuric acid tested for alkenes expected in cholesterol.
White precipitate shows the presence of chloride (Cl-). Chloride anion equation: HCl(aq) + AgNO3 (aq) → HNO3 (aq) + AgCl(s). The nitrate anion test involves cooling a mixture containing 1 mL of test solution and 3mL 18M H2SO4. 2mL is poured down the inner test tube side and the presence of a brown ring shows nitrate (NO3-) to be present. The carbonate anion test mixes 1 mL of test solution and drops of 6M HCl.
Abstract The interaction at equilibrium between acids and bases during a titration can be used to determine several characteristics of the acid or the base. In this experiment 0.05 M of KHP titrate with the strong base NaOH. From the plot of pH versus the volume of sodium hydroxide added was found that acid ionization constant Ka for KHP at half point was equal to 8.3176x10-6, also the dissociation constant Kb for conjugate base of weak acid was equal to 1x10-9. This value was established by observing the pH versus volume of NaOH graph. The equivalence point of titration occurred at a volume of 31 mL 0.081M NaOH (aq).
Ashley Peccatiello Experiment 7 – Dehydration of 2-Methylclyclohexanol, Tests for Unsaturation, and Gas Chromatography Date Performed: October 25, 2012 Date Written: October 29, 2012 Purpose: To dehydrate 2-methylclyclohexanol to obtain two isomers. To separate the products by simple distillation. To analyze the sample by introducing the technique of gas chromatography and unsaturation tests. Reaction: Figure 1. Overall reaction of the acid-catalyzed dehydration of 2-methylcyclohexanol Figure 2.