Monitoring Acid-Base Titrations with a Ph Meter

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William Flores-Paz Monitoring Acid-Base Titrations with a pH meter October 30, 2013 Introduction The purpose of this experiment was to record the volume of HCl and acetic acid with a NaOH with a known molarity. This data would allow us to create a graph so we could compare the two titration curves. We would then use these curves to calculate the unknown molarities. HCl + NaOH >H2O + NaCl This equation shows the relationship between the acid and the base then the reaction goes forward and they are titrated creating salt and water. This particular reaction is a strong acid and a strong base which means that when the reaction reaches the equivalence point, the moles of the acid and the base are equal and the solution is neutral so the pH should be around 7.0 depending on the final volume of each solution. To get this data, we will titrate an HCl solution with NaOH solution of which is a known concentration. We will record the initial and final reading of the NaOH while we record the pH of the titrated solution in the beaker. We will repeat this process with a solution of acetic acid which is a weak acid with NaOH and record the initial and final reading of NaOH and the pH of the solution in the beaker. Procedure Preview Calibrate the pH meter. Fill buret with standardized NaOH solution Titrate HCL solution with standardized NaOH solution, monitoring the pH as titrant added. Titrate HC2H3O2 solution with standardized NaOH solution, monitoring the pH as titrant added. Calibrating the pH meter Transfer 50mL of the buffer solution into a 150mL beaker. Carefully immerse the electrons in the solution. Turn the function knob to “pH”. Turn the standardize knob until the meter indicate the exact pH of the buffer solution. Record the pH at which the meter is standardized. Titrating HCl solution with NaOH solution Obtain 25mL of 0.100M HCL solution

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