In another flask 50-mL of ice water was deposited with three-drop phenolphthalein. Using a volumetric pipet 50-mL of the 1-bromopropane was added into the empty flask in the bath. By the same method 50-mL of potassium hydroxide was delivered to the same flask while swirling the contents and remaining in the water bath. A 10-mL aliquot was immediately removed from the mixture and added to the ice water containing the phenolphthalein. When the pipet was half emptied into the ice water a timer was started.
The watch glass was removed with the beaker tongs. Using a rubber bulb and a stirring rod to stir the solution continuously, 15.00mL of .25M BaCl2 solution was added to the solution in the beaker. The watch glass is replaced and the solution is keep hot but not boiling for 15 minutes. The precipitate was allowed to settle. When the liquid above the precipitate was clear, the solution was tested for completeness of precipitation when a few drops of BaCl2 solution were added from a pipette.
A voltmeter was used to measure the electrical resistance of different solutions. * Experiment and Observation: The plastic and glassware used in this experiment was thoroughly washed with hot water and rinsed with distilled water. * * Part I: Preparation of Standard Phosphate Solutions 1. 1.0 ppm standard: 1.00 mL of 10.0 ppm phosphate solution was placed in a 25 mL graduated cylinder and diluted to exactly the 10 mL mark with distilled water then poured into a plastic cup labeled 1. Cylinder was rinsed with distilled water.
The second experiment, procedure 1, combined [Co(NH3)5 (H2O)]Cl2 (0.0060M, 1.52g) and (25mL) of distilled water to an 125mL Erlenmeyer flask. The flask was gently heated (dial 5-6) and stirred until all the compound was dissolved. The heated solution was then vacuum filtered through a fritted funnel and the filtrate was cooled in an ice bath until the
Then, it was removed and one drop of room temperature water was added. The tube was swirled. The process was repeated until no boiling occurred. 24 mL of room temperature water were added and the mixture was stirred. Once the crystals began to form, the tube was placed in a beaker filled with ice water.
Procedure 1. Begin to prepare an EDTA solution. Weigh out 3.62-3.64 g of NaH2EDTA and record exact mass. Add the weighed amount to a 250 ml volumetric funnel carefully using a funnel Wash the funnel with water to ensure all of the solid is delivered to the flask Add 100-200 ml of water and mix. Enough water should be added so that the flask is full to the 250 ml mark Tightly wrap the top of the flask with a Parafilm when finished 2.
Compare the MPs of the once recrystallized and the twice recrystallized trimyristin. After the hydrolysis has proceeded for 45 minutes, allow the flask to cool to RT and pour the contents into a 50 mL beaker containing 8 mL of water. Carefully, in the hood, add dropwise with stirring, 2 mL of concentrated HCl (caution: corrosive liquid/noxious vapors). Myristic acid should precipitate. Cool the beaker in ice water for 10 min, with stirring, and collect the solid by vacuum filtration on a small Hirsch funnel.
Purpose: The purpose of this experiment is to measure the rate of increase (slope) of the water given two different starting points to the boiling point of 212 degree Fahrenheit in the span of time. The rate of increase in water temperature as it is heated given all control variables are the same such as one quart aluminum pot holding three cups of refrigerate and room temperature water. The study is to conduct weather if both types water will have the same slop of increase. Procedure: The first step was to fill a jug full of water and leave it in the fridge to cool down overnight and another jug full of water so that it becomes part of room temperature. Before the experiment, take out the fridge water and measure out three cups and pour it into the one quart pot and measure the water temperature before placing it on the stove.
DNA Extraction Aim: To extract DNA from a carrot using house hold products. Method: * Step 1 – Pour 60 ml (¼ cup) of clear alcohol into a glass. Place the glass into the bowl of iced water to chill, then set aside. * Step 2 – Pour 120 ml (½ cup) of tap/distilled water into the measuring cup with the salt. Add 30 ml (2 tablespoons) of clear detergent and mix carefully until the salt is dissolved.
Reaction : CO2+H2O → H2CO3 Technique : I will prepare a bowl that can fit 1000cc water. Then measure the initial temperature of the water using Pasco sensor first. Then, I will use insulated gloves to put one dry ice every 30 seconds and see the temperature change. I will do this continuously until 300 seconds then I stop. Variable : Control - Water, 1000cc Independent - Dry ice amount, 1-10 Dependent - Temperature Background Information: Dry ice is frozen carbon dioxide, Co2, which can make lots of fascinating experiment.