Magic marker inks are often mixtures of several compounds. Paper chromatography is a common method of separating various components of a mixture. After separation, you can observe the different colors that make up a particular color of magic marker ink. You can also calculate a ratio Rf, which compares how far each compound traveled to how far each solvent (substance that dissolves another substance) traveled during the experiment. Rf = Ds/Df Ds = Distance traveled by the compound Df = Distance traveled by the solvent Materials: coffee filter, tape, isopropyl alcohol (rubbing alcohol), water, 3 different color magic markers (not permanent); 3 identical tall, narrow drinking glasses; metric ruler, 3 pencils Pre-lab Questions: List one extensive and one intensive property of marker ink.
ABSTRACT Isopropyltoluene isomers were synthesized through the friedel-crafts alkylation of toluene with 2-chloropropane in the presence of aluminum chloride as a catalyst. Through extraction of the distillate with water and 5% NaHCO3, followed by a fractional vacuum distillation, the desired aromatic organic compound was isolated. Infrared Spectroscopy and Gas Chromatography were used to analyze the composition, purity and to confirm the identity of the prepared product. The sample weighed approximately 2.66g, which reflected a low yield at 47%. However, from the GC the area % (also known as percent purity) was 91.8%, which indicates that a very pure product was obtained.
3. Dilute acid solution: Use 0.01–0.1 M hydrochloric acid. 4. Sodium hydroxide solution: Use 0.01 M sodium hydroxide, 0.40 g/L. 5.
Also a very pale purple tint formed. Acid test: Added 2 mL of 1M NaOH- no Physical change was observed. Base test: Added 2 mL of .17M Acetic acid- No physical change observed. Table: Zinc (g) | Iodine (g) | Deionized water (mL) | Weight of boiling tube (g) | 1M NaOH(mL) | .17M Acetic acid (mL) | 2 | 2.01 | 5 | 40.73 | 2 | 2 | 2. Answer to focus question: Since it is amphoteric, it will act as an acid if reacts with base and act as a base when reacts with acid.
Referring to a solubility table, name at least four ionic compounds that could be dissolved in water to make a solution containing aqueous copper (II) ions. b. Write a balanced chemical equation for the reaction of aluminum with one of the compounds you suggested in a). c. Write the total ionic equation for the reactions. d. Write the total net ionic equation for the reactions.
Observations of Physical and Chemical Changes Purpose- The different tests can interact and change in different ways, by doing these tests we can figure out if it could be either a physical change or chemical change by observing the test and chemicals. Procedure- In test one, you mixed a small amount of iodine in each test tube and fill one of the with just tap water and the second one with hexane. Test two, you measure 5 grams of barium hydroxide and same measurement of ammonium chloride and stir with a stirring rod. Test three, you use a small piece of steel wool and you place it over a Bunsen burner using tongs and observe what you see. Test four, by using a plastic bag, you place a spoon full of calcium chloride in one corner and
Results APPEARANCES OF MATERIALS USED Substance Physical Appearance Zinc Carbonate White; powderish Calcium Hydroxide White; powderish; like zinc carbonate 3 M HCL Clear liquid, resembles water 20 mesh granular zinc Grey, metallic, shiny 3% hydrogen peroxide Clear liquid; resembles water Manganese dioxide Very dark grey, black and powdery Copper sulfate Blue, crystalline in structure. Sky blue Zinc iodide Very dark purple, shiny and crystalline in structure 0.1 M acetic acid Clear liquid, resembles water Zinc oxide Very white powdery substance RAW RESULTS Data Specifided (Page 112 CRC handbook) Raw data Volume of Gas Collection Bottle (Average of 3 Trials) 14.04mL Mass of boiling tube (empty) 41.57g Mass of boiling tube with zinc carbonate 43.42g Mass of zinc carbonate 1.75g Volume of water in gas collection bottle after reaction 78.5mL Volume of gas product collected 185.2mL Mass of solid product with boiling tube after reaction 1.11g QUALITATIVE TEST RESULTS Group # Test Observation: Standard Positive/Negative Observation: Experimental Positive/Negative 1 H2 HCL + Zinc bubbling + flaming stick POP! + + flaming splint no POP - 2 CO2 Turned cloudy + Negated from experiment Negated from experiment 3 O2 MgO2 + Hydrogen Peroxide bubbling. Glow stick re-ignited + + wooden splint; glowing stick went out - 4 H2) Added 1 pea size CuSulfate + 1 drop of deionized water; blue, positive + Copper sulfate did not change color when put into wet filter paper - 5 Zn (OH)2 Zinc iodide + 3mL H2O Clear suspension + Visual inspection; cloudy. Acid test= solid + 3M Acetic acid cloudy + 6 ZnO ZnO + Heat yellow Zn Cooled White + ZnCO3 + heat yellow solid.
Strychnine Strychnine is also known as Strychnos, Strychnidin-10-one, Stricnina, Sanaseed, Strychnin, NSC5365, Certox, 57-24-9 and Dolco mouse cereal. It is an odourless substance that appears in forms of white crystals or powder. Its taste is bitter, density equals 1.42g/cm3, melting point is 284-286 °C and boiling point is 559.9°C . It is a stable compound which is incompatible even with strong oxidizing agents. Strychnine with its molecular formula C21H22N2O2 weights 334.41158 [g/mol].
25 cm3 of a solution of sodium hydroxide reacts with 15 cm3 of 0.1 mol/dm3 HCl. What is the molar concentration of the sodium hydroxide solution? 4. Succinic acid has the formula (CH2)n(COOH)2 and reacts with dilute sodium hydroxide as follows: (CH2)n(COOH)2 + 2NaOH → (CH2)n(COONa)2 + 2H2O 2.0 g of succinic acid were dissolved in water and the solution made up to 250 cm3. This solution was placed in a burette and 18.4 cm3 was required to neutralise 25 cm3 of 0.1 moldm-3 NaOH.
In this lab we synthesized and analyzed potassium aluminum sulfate (KAl(SO4)12H2O) using a multiple different tests. These test included flame test, melting point, potassium test, sulfate test, and aluminum test. We also determined the number of waters of hydration in Alum. Experimentally and empirically potassium aluminum sulfate is a dodecahydrate (4). The purpose of the laboratory is to determine the number of waters of hydration in aluminum potassium sulfate as well as the purity of the Alum we produce.