Calculate the molarity of the original vinegar solution and its concentration in gdm-3, given that it reacts with NaOH in a 1:1 ratio. 7. 2.5 g of a sample of ethanedioic acid, H2C2O4.nH2O, was dissolved in water and the solution made up to 250 cm3. This solution was placed in a burette and 15.8 cm3 were required to neutralise 25 cm3 of 0.1 moldm-3 NaOH. Given that ethanedioic acid reacts with NaOH
For example, the reaction |BaCl2•2H2O ( BaCl2 + 2H2O |(2) | is reversible, and if water is added to the anhydrous salt BaCl2, formation of BaCl2•2H2O takes place: |BaCl2 + 2H2O ( BaCl2•2H2O |(3) | The reaction of dehydration of hydrated ferrous sulfate |FeSO4•7H2O ( FeSO4 + 7H2O |(4)
We added anhydrous Sodium Sulfate as a drying agent. To complete, we distilled the cyclohexene and collected the product. Knowing this data, we determined the yield % which is 58.5%. This experiment features the dehydration of cyclohexanol and produce cyclohexene. The acid catalyzed dehydration of cyclohexanol with distillative removal of the resulting cyclohexene from the reaction mixture
h) A way to make hard water softer is to put an sodium nitrate and create a precipitate to mellow out the reaction. Another way of making it softer is by removing the calcium ions one way of doing that is by boiling the solution to take out some of the ions. Conclusion: Overall, we determined that sodium carbonate, Na2CO3, is the anion that can be used to precipitate the most metal cations. Also, we learned that the anion sodium chloride, NaCl, could be used to remove silver ions from solutions. The stuff that I found interesting was that how many colours you can get when you mix the cations and anions
Purpose of the Experiment: To produce diphenylmethanol from the reduction of benzophenone by using sodium borohydride as a reducing agent. To check purity of a product by using thin layer chromatography (TLC) and by performing a melting point. Introduction: The key step in the reduction of a carbonyl compound by either lithium aluminium hydride or sodium borohydride is the transfer of a hydride ion from the metal to the carbonyl carbon. In this transfer the hydride ion acts as nucleophile. The mechanism for the reduction of a ketone by sodium borohydride: (1) Method (Based on Chemistry Laboratory Manual): 1.
In the experiment a secondary alcohol (cyclohexanol) is heated with acid (phosphoric acid). A carbocation is generated by the loss of water from cyclohexanol because of the protonated alcohol. Loss of hydrogen ion from the carbocation will give the desired alkene (cyclohexene). Fractional distillation is used to separate liquids that have different boiling points that are relatively close together. By using this method of distillation a mixture is heated to a temperature at which several fractions of the compound is evaporated the distillate is then condensed and collected.
EXPERIMENT ( 3 ) Topic : The preparation of Phenyl Benzoate from benzoyl chloride Introduction : The preparation of phenyl benzoate (ester) from phenol and benzoyl chloride is an esterification. In this experiment, you are requested to prepare and purify phenyl benzoate by some techniques. Chemicals : Phenol, Benzoyl chloride, Dilute NaOH, Methanol Procedures : 1. Dissolve 1 g phenol in 15 cm3 dilute NaOH using a 50 cm3 quickfit flask. 2.
A binding material can be separated by dissolving the tablet in ether since three active ingredients are soluble. Then, aqueous K2HPO4 and KOH are used to extract the ether solution with the conjugate base of the Aspirin layer and the conjugate base of the Acetaminophen, respectively. The caffeine can be isolated from the left over layer by evaporating the ether. Two separated solutions form solid by acidifying with HCl and the solid residue can be collected by vacuum filtration. According to the Revell's lab experiment, aspirin, acetaminophen, caffeine recoveries are 60% or higher, <10% and <5%, respectively.
Carboxylic acids, their derivatives and Amines Experiment 1 5 cm3 of dilute ethanoic acid with : | Turned: | A few drops of U.I solution | Pinky red | Strip of magnesium | Effervescence | ½ spatula of sodium hydrogen carbonate | effervescence | ¼ spatula of Copper (2) oxide | Turns brown/black then goes deep blue | 3cm3 of ethanol + Conc H2SO4 + sodium carbonate solution | Smelt like modelling glue | Equations: 1. A) CH3COOH -> CH3COO- + H+ B) 2CH3COOH + Mg ---> (CH3COO)2 Mg + H2 C) CH3COOH +NaHCO3--->NaCH3COO + CO2 +H2O D) 2CH3COOH + CuO ---> (CH3COO) 2Cu + H2O E) Method 1. Set up a testube rack, with 5 test tubes. 2. Within each testube add 5cm3 of ethanoic acid 3.
Questions: 1. Write an equation that explains the solubility of diethylamine in water (CH2CH3)2NH (CH2CH3)2N+ (CH2CH3)2NOH (CH2CH3)2NOHO- (CH2CH3)2NO- 2. Write an equation for the reaction of dibutylamine with HCl and for treatment of the product with NaOH 3. For the reaction of butylamine with nitrous acid a) Write structural formula of the diazonium ion formed i. CH3CH2CH2CH2-N- b) From