Pour all the filtrate and washings into a 250cm3 volumetric flask. Make up to 250cm3 with 1.0mol dm-3 sulphuric acid(VI) acid. Stopper the flask and invert several times to thoroughly mix the solution. 5. Fill the burette with 0.005mol dm-3 potassium manganate(VII) solution.
12. Place a paper towel over the drain, pour the content of the well plate, throw the paper towel and rinse the well plate. DATA, OBSERVATIONS, AND CALCULATIONS: Data Table: Oxidation - Reduction | | Reactions | Mg in Na2SO4 | Bubbles | Zn in MgSO4 | Small bubbles | Pb in Zn(NO3)2 | Dark lead changed into lighter color | Pb in FeCl3 | Changed the lead into slight green yellow | Fe in CuSO4 | Changed the iron into orange color | Note: I added more than 10 drops to make sure that the pieces are well covered. QUESTIONS: A. Based on your observations make an activity series of the metals used.
Measure and record the mass of the test tube and metal. 5. Place the test tube containing the metal into the beaker of water and continue heating (10 min). Leave the test tube in the boiling water bath while you complete steps 6 and 7. 6.
Stirring carefully and observe the color of the hydrate until it changes to a consistent white color, then the Copper(II) Sulfate is dehydrated. 6. Turn off the burner, and wait to cool down the material. 7. Carefully determine the mass of the Copper(II) Sulfate, crucible, and lid.
Record the temperature of the water in the Calorimeter and the temperature of the boiling water. 7. Quickly pour the metal into the Calorimeter. 8. Stir the Calorimeter slowly with the thermometer.
17. Press START and turn on the stir bar. 18. After 10 seconds have elapsed, add hot water sample 19. Press STOP when the thermograph stabilizes 20.
Fill a 10 mL graduated cylinder with ≈ 7mL if water c. Fill a 1000 mL beaker with ≈ 750 mL of water d. Invert the graduated cylinder into the beaker. Add water to the beaker to completely submerge cylinder. e. Measure the difference between the height of the water in the graduated cylinder and the height of the water in the beaker. f. g. Record the barometric pressure in mmHg. Heat the water via Bunsen burner to 80°C.
After heating, the mixture was cooled to room temperature and filtered by vacuum filtration into a fritted funnel to yield a purple product. The product was washed 3 times with (5mL) portions of chilled 6M HCL, then Ethanol, and lastly with acetone. The resulting product was placed into a vial and left to dry in a vacuum desiccator for 1 week and weighed the next week. The yield was 6.029g. The second experiment, procedure 1, combined [Co(NH3)5 (H2O)]Cl2 (0.0060M, 1.52g) and (25mL) of distilled water to an 125mL Erlenmeyer flask.
Put that magnesium strips into the conical flask which contains 50 cm3 of 0.2 M hydrochloric acid. 6. Immediately close the conical flask with stopper and start stopwatch. 7. Record the volume of gas in burette in every 30 seconds for 5 minutes.
The watch glass was removed with the beaker tongs. Using a rubber bulb and a stirring rod to stir the solution continuously, 15.00mL of .25M BaCl2 solution was added to the solution in the beaker. The watch glass is replaced and the solution is keep hot but not boiling for 15 minutes. The precipitate was allowed to settle. When the liquid above the precipitate was clear, the solution was tested for completeness of precipitation when a few drops of BaCl2 solution were added from a pipette.